Fe₃(CO)9{(C₆H₅)C₂(C₆H₅)}

Base Information

Chemical Name:Fe₃(CO)9{(C₆H₅)C₂(C₆H₅)}
CAS No.:12171-93-6
Molecular Formula:C₂₃H₁₀Fe₃O₉
Molecular Weight:597.868
Hs Code.:

Fe<sub>3</sub>(CO)9{(C<sub>6</sub>H<sub>5</sub>)C<sub>2</sub>(C<sub>6</sub>H<sub>5</sub>)}

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Chemical Property of Fe₃(CO)9{(C₆H₅)C₂(C₆H₅)}

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Technology Process of Fe₃(CO)9{(C₆H₅)C₂(C₆H₅)}

There total 3 articles about Fe₃(CO)9{(C₆H₅)C₂(C₆H₅)} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: P(C₆H₅)4⁽¹⁺⁾*Fe₃(CO)9H(C₂(C₆H₅)2)^(1-)={P(C₆H₅)4}{Fe₃(CO)9H(C₂(C₆H₅)2)}

: 12171-93-6
Fe₃(CO)9{(C₆H₅)C₂(C₆H₅)}

Guidance literature:: With silver perchlorate; In dichloromethane; benzene; under N2; addn. of AgClO4 in benzene with stirring to Fe-complex in CH2Cl2/benzene (5/1), stirred for 15 min; evapn., residue extd. (hexane), crystn. (hexane);
DOI:10.1016/0022-328X(86)84010-4

Reference yield: 20.0%

: 17685-52-8
triiron dodecarbonyl

: 501-65-5
diphenyl acetylene

: 12171-93-6
Fe₃(CO)9{(C₆H₅)C₂(C₆H₅)}

Guidance literature:: In hexane; mixt. of Fe3(CO)12 and alkyne in 1:1 mol. ratio in n-hexane was heated at reflux under N2 for 6 h; chromy. on TLC plates (SiO2, eluant petroleum ether-Et2O);

Reference yield: 15.0%

: P(C₆H₅)4⁽¹⁺⁾*Fe₃(CO)9H(C₂(C₆H₅)2)^(1-)={P(C₆H₅)4}{Fe₃(CO)9H(C₂(C₆H₅)2)}

: 12171-93-6
Fe₃(CO)9{(C₆H₅)C₂(C₆H₅)}

: 2Fe⁽¹⁺⁾*6CO*C₆H₄CHCC₆H₅^(2-)=Fe₂(CO)6(C₆H₅)CC(C₆H₅)

Guidance literature:: With [(C₂H₅)3O]BF₄; In dichloromethane; under N2; 1/1 mixt. of Fe-complex and (Et3O)BF4 in min. amt. of CH2Cl2 stirred (12 h, room temp.); evapn., residue extd. (pentane), evapn. (reduced pressure), chromy. (silica gel, hexane);
DOI:10.1016/0022-328X(86)84010-4