5-phenylthiomethyl-2tetrahydrofuran

Base Information

Chemical Name:5-phenylthiomethyl-2tetrahydrofuran
CAS No.:92631-31-7
Molecular Formula:C₂₅H₂₄OS₂
Molecular Weight:404.597
Hs Code.:

5-phenylthiomethyl-2<phenylthio(p-tolyl)methylene>tetrahydrofuran

Synonyms:

Suppliers and Price of 5-phenylthiomethyl-2tetrahydrofuran

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-phenylthiomethyl-2tetrahydrofuran

Chemical Property:

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Technology Process of 5-phenylthiomethyl-2tetrahydrofuran

There total 4 articles about 5-phenylthiomethyl-2tetrahydrofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 7.1%

: 92631-30-6
2-trimethylsilyloxy-1-p-tolylhexa-1,5-diene

: 931-59-9
benzenesulfenyl chloride

: 92631-31-7
5-phenylthiomethyl-2tetrahydrofuran

: 92631-32-8
5-chloro-1,6-bis(phenylthio)-1-p-tolylhexan-2-one

Guidance literature:: In dichloromethane; for 12h; Ambient temperature;

Reference yield:

: 104-09-6
4-methylphenylacetaldehyde

: 92631-31-7
5-phenylthiomethyl-2tetrahydrofuran

Guidance literature:: Multi-step reaction with 4 steps

1: 87 percent / tetrahydrofuran / 1 h / Ambient temperature

2: 86.7 percent / pyridinium chlorochromate / CH₂Cl₂ / 1.5 h / Ambient temperature

3: 86 percent / triethylamine / dimethylformamide / 18 h / Heating

4: 33 percent / CH₂Cl₂ / 12 h / Ambient temperature

With triethylamine; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 92631-27-1
6-p-tolylhex-1-en-5-ol

: 92631-31-7
5-phenylthiomethyl-2tetrahydrofuran

Guidance literature:: Multi-step reaction with 3 steps

1: 86.7 percent / pyridinium chlorochromate / CH₂Cl₂ / 1.5 h / Ambient temperature

2: 86 percent / triethylamine / dimethylformamide / 18 h / Heating

3: 33 percent / CH₂Cl₂ / 12 h / Ambient temperature

With triethylamine; pyridinium chlorochromate; In dichloromethane; N,N-dimethyl-formamide;