Cr₂(2,6-bis(phenylamino)pyridine)4*toluene

Base Information

• Chemical Name: Cr₂(2,6-bis(phenylamino)pyridine)4*toluene
• CAS No.: 347840-33-9
• Molecular Formula: C₇H₈*C₆₈H₅₆Cr₂N₁₂
• Molecular Weight: 1237.41
• Mol file: 347840-33-9.mol

Synonyms:

Chemical Property of Cr₂(2,6-bis(phenylamino)pyridine)4*toluene

Chemical Property:

Purity/Quality:

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Technology Process of Cr₂(2,6-bis(phenylamino)pyridine)4*toluene

There total 1 articles about Cr₂(2,6-bis(phenylamino)pyridine)4*toluene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

chromium dichloride + hexane (110-54-3) + N2,N6-diphenylpyridine-2,6-diamine (5051-97-8) + toluene (108-88-3,15644-74-3,16713-13-6) → Cr2(2,6-bis(phenylamino)pyridine)4*toluene (347840-33-9) + Cr2(2,6-bis(phenylamino)pyridine)4*hexane (348637-11-6)

Guidance literature:

With MeLi; In tetrahydrofuran; ligand was dissolved in THF, MeLi at -78°C was added under N2, warmed to room temp., CrCl2 was added, stirred at room temp. overnight; filtered, toluene was added, filtered, layer of hexane was added, 2 wks,dried under vac., ppt. was washed with ether, dissolved in THF, layered with hexane, 9 ds, elem. anal.;

DOI:10.1021/ic001376g

upstream raw materials:

hexane

N²,N⁶-diphenylpyridine-2,6-diamine

toluene