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Technology Process of (CH3C6H4NC(CH3)CHC(CH3)NC6H4CH3)3Yb

(CH3C6H4NC(CH3)CHC(CH3)NC6H4CH3)3Yb

Base Information
  • Chemical Name:(CH3C6H4NC(CH3)CHC(CH3)NC6H4CH3)3Yb
  • CAS No.:1239498-29-3
  • Molecular Formula:C57H63N6Yb
  • Molecular Weight:1005.21
  • Hs Code.:
(CH<sub>3</sub>C<sub>6</sub>H<sub>4</sub>NC(CH<sub>3</sub>)CHC(CH<sub>3</sub>)NC<sub>6</sub>H<sub>4</sub>CH<sub>3</sub>)3Yb

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Chemical Property of (CH3C6H4NC(CH3)CHC(CH3)NC6H4CH3)3Yb
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Technology Process of (CH3C6H4NC(CH3)CHC(CH3)NC6H4CH3)3Yb

There total 1 articles about (CH3C6H4NC(CH3)CHC(CH3)NC6H4CH3)3Yb which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

ytterbium(III) chloride
10361-91-8

ytterbium(III) chloride

Li<sup>(1+)</sup>*CH<sub>3</sub>C<sub>6</sub>H<sub>4</sub>NC(CH<sub>3</sub>)CHC(CH<sub>3</sub>)NC<sub>6</sub>H<sub>4</sub>CH<sub>3</sub><sup>(1-)</sup>=LiCH<sub>3</sub>C<sub>6</sub>H<sub>4</sub>NC(CH<sub>3</sub>)CHC(CH<sub>3</sub>)NC<sub>6</sub>H<sub>4</sub>CH<sub>3</sub>

Li(1+)*CH3C6H4NC(CH3)CHC(CH3)NC6H4CH3(1-)=LiCH3C6H4NC(CH3)CHC(CH3)NC6H4CH3

(CH<sub>3</sub>C<sub>6</sub>H<sub>4</sub>NC(CH<sub>3</sub>)CHC(CH<sub>3</sub>)NC<sub>6</sub>H<sub>4</sub>CH<sub>3</sub>)3Yb
1239498-29-3

(CH3C6H4NC(CH3)CHC(CH3)NC6H4CH3)3Yb

Guidance literature:
In tetrahydrofuran; (Ar), slurry of YbCl3 in THF treated with 3 equiv. of ligand in THF at room temp., stirred at 60°C for 24 h; evapd.(vac.), crystd.(hexane/toluene) at room temp., elem. anal.;
DOI:10.1002/ejic.201000156
upstream raw materials:

ytterbium(III) chloride

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