tert-butyl 4-Methylideneazepane-1-carboxylate

Base Information

Chemical Name:tert-butyl 4-Methylideneazepane-1-carboxylate
CAS No.:790705-08-7
Molecular Formula:C12H21NO2
Molecular Weight:211.3
Hs Code.:2933990090
Mol file:790705-08-7.mol

Synonyms:tert-butyl 4-methylene-azepan-1-carboxylate;tert-Butyl 4-methyleneazepane-1-carboxylate;

Suppliers and Price of tert-butyl 4-Methylideneazepane-1-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
tert-Butyl4-methyleneazepane-1-carboxylate 95+%
1g
$ 772.00

Chemenu
tert-butyl4-methyleneazepane-1-carboxylate 95%
1g
$ 729.00

American Custom Chemicals Corporation
TERT-BUTYL-4-METHYLENEAZEPANE-1-CARBOXYLATE 95.00%
1G
$ 2304.23

Alichem
tert-Butyl4-methyleneazepane-1-carboxylate
1g
$ 678.24

Total 11 raw suppliers

Chemical Property of tert-butyl 4-Methylideneazepane-1-carboxylate

Chemical Property:

PSA：29.54000
LogP:2.90150

Purity/Quality:

99% ^*data from raw suppliers

tert-Butyl4-methyleneazepane-1-carboxylate 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of tert-butyl 4-Methylideneazepane-1-carboxylate

There total 3 articles about tert-butyl 4-Methylideneazepane-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 188975-88-4
tert-butyl 4-oxoazepane-1-carboxylate

: 2065-66-9
methyl-triphenylphosphonium iodide

: 790705-08-7
4-methylene-azepane-1-carboxylic acid tert-butyl ester

Guidance literature:: methyl-triphenylphosphonium iodide; With n-butyllithium; In tetrahydrofuran; diethyl ether; at 0 ℃; for 1h;

tert-butyl 4-oxoazepane-1-carboxylate; In tetrahydrofuran; diethyl ether; at 0 ℃;
DOI:10.1002/anie.202103278

Reference yield: 85.0%

: 188975-88-4
tert-butyl 4-oxoazepane-1-carboxylate

: 1779-49-3
Methyltriphenylphosphonium bromide

: 790705-08-7
4-methylene-azepane-1-carboxylic acid tert-butyl ester

Guidance literature:: Methyltriphenylphosphonium bromide; With n-butyllithium; In tetrahydrofuran; hexane; at -14 ℃; Inert atmosphere;

tert-butyl 4-oxoazepane-1-carboxylate; In tetrahydrofuran; hexane; at 20 ℃;

Reference yield: 67.0%

: 790705-08-7
4-methylene-azepane-1-carboxylic acid tert-butyl ester

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 5 - 10 ℃; for 1h; Inert atmosphere;

In tetrahydrofuran; at 5 - 20 ℃; for 12h; Inert atmosphere;