W(CO)4(P(C₆H₅)2CH(COC₆H₅)P(C₆H₅)2)

Base Information

Chemical Name:W(CO)4(P(C₆H₅)2CH(COC₆H₅)P(C₆H₅)2)
CAS No.:82328-15-2
Molecular Formula:C₃₆H₂₆O₅P₂W
Molecular Weight:784.397
Hs Code.:

W(CO)4(P(C<sub>6</sub>H<sub>5</sub>)2CH(COC<sub>6</sub>H<sub>5</sub>)P(C<sub>6</sub>H<sub>5</sub>)2)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of W(CO)4(P(C₆H₅)2CH(COC₆H₅)P(C₆H₅)2)

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Technology Process of W(CO)4(P(C₆H₅)2CH(COC₆H₅)P(C₆H₅)2)

There total 2 articles about W(CO)4(P(C₆H₅)2CH(COC₆H₅)P(C₆H₅)2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 41830-14-2
tetracarbonyl-bis(diphenylphosphino)methane-tungsten(0)

: 98-88-4
benzoyl chloride

: 82328-15-2
W(CO)4(P(C₆H₅)2CH(COC₆H₅)P(C₆H₅)2)

Guidance literature:: With n-butyllithium; In diethyl ether; treatment a soln. of complex with BuLi followed by benzoyl chloride;
DOI:10.1039/c39820000286

Reference yield: 80.0%

: 109-72-8,29786-93-4
n-butyllithium

: 41830-14-2
tetracarbonyl-bis(diphenylphosphino)methane-tungsten(0)

: 98-88-4
benzoyl chloride

: 82328-15-2
W(CO)4(P(C₆H₅)2CH(COC₆H₅)P(C₆H₅)2)

Guidance literature:: In diethyl ether; benzene; soln. of LiBu(n) in Et2O was added to a soln. of W-complex in benzene, mixt. was stirred at ca. 20°C for 2 h, cooled to 0°C and ligand added, mixt. was stirred at ca. 20°C for 4 h; ppt. was formed from CHCl3-MeOH; elem. anal.;

Reference yield: 92.0%

: 82328-15-2
W(CO)4(P(C₆H₅)2CH(COC₆H₅)P(C₆H₅)2)

: 98-88-4
benzoyl chloride

: 91382-22-8
W(CO)4(P(C₆H₅)2)2CCC₆H₅(OCOC₆H₅)

Guidance literature:: With pyridine; In benzene; mixt. of W-complex and pyridine in benzene was treated with ligand, mixt. was refluxed gently for 10 min, mixt. was cooled to ca. 20°C, H2O was added; ppt. was formed from CHCl3-MeOH; elem. anal.;