C₄₄H₃₀ClInN₄

Base Information

• Chemical Name: C₄₄H₃₀ClInN₄
• CAS No.: 36522-28-8
• Molecular Formula: C₄₄H₃₀ClInN₄
• Molecular Weight: 765.022
• Mol file: 36522-28-8.mol

Synonyms:

Chemical Property of C₄₄H₃₀ClInN₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₄H₃₀ClInN₄

There total 4 articles about C₄₄H₃₀ClInN₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

(TPP)In(C2H5) (63036-65-7) → (5,10,15,20-tetraphenylporphyrinato)(chloro)indium(III) (36522-28-8,63128-70-1)

Guidance literature:

With hydrogenchloride; air; In benzene; Irradiation (UV/VIS); irradiation of aerated soln. by sunlight for 2 days; evapn. of the benzene; residue was dissolved in an ethanol soln. of HCl; identification by IR and UV;

DOI:10.1021/j100408a031

Reference yield: 60.0%

5,10,15,20-tetraphenyl-21H,23H-porphine (917-23-7,20998-75-8) + indium trichloride trihydrate (22519-64-8) → (5,10,15,20-tetraphenylporphyrinato)(chloro)indium(III) (36522-28-8,63128-70-1)

Guidance literature:

In further solvent(s); prepn. according to T. N. Lomova et al., Zh. Obshch. Khim., 59, 2317 (1989) by coordintion of ligand with InCl3*3H2O in boiling phenol; isolated and purified by multiply washing of cooled mixt. in CHCl3 with warm H2O and by double chromatographing on Al2O3 column (CHCl3 as eluent); elem. anal.;

DOI:10.1134/S0036024409060077

Reference yield: 48.0%

indium(III) chloride + 5,15,10,20-tetraphenylporphyrin (917-23-7,20998-75-8) → C44H30ClInN4 (36522-28-8,63128-70-1)

Guidance literature:

With sodium acetate; In acetic acid; at 110 ℃; for 30h;

DOI:10.1039/c4cc02759k

upstream raw materials:

5,10,15,20-tetraphenyl-21H,23H-porphine

indium trichloride trihydrate

(TPP)In(C₂H₅)

(chloro)indiumtetraphenylchlorin

Downstream raw materials:

{(5,10,15,20-tetraphenylporphyrinato)indium(III)}tetracarbonylcobalt

(C₄₄H₂₈N₄)In(C₆F₅)

(C₄₄H₂₈N₄)In(C₆F₄H)

(C₂₀N₄H₈(C₆H₅)4)InMn(CO)5