2-AMINO-4,6-DIMETHOXYPYRIDINE

Base Information

• Chemical Name: 2-AMINO-4,6-DIMETHOXYPYRIDINE
• CAS No.: 256642-28-1
• Molecular Formula: C7H10N2O2
• Molecular Weight: 154.17
• Mol file: 256642-28-1.mol

Synonyms:2-AMINO-4,6-DIMETHOXYPYRIDINE

Chemical Property of 2-AMINO-4,6-DIMETHOXYPYRIDINE

Chemical Property:

• Boiling Point: 287.2oC at 760 mmHg
• Flash Point: 127.5oC
• PSA: 57.37000
• Density: 1.159g/cm3
• LogP: 1.26220

Purity/Quality:

98%min ^*data from raw suppliers

2-AMINO-4,6-DIMETHOXYPYRIDINE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-AMINO-4,6-DIMETHOXYPYRIDINE

There total 1 articles about 2-AMINO-4,6-DIMETHOXYPYRIDINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

nicosulfuron (111991-09-4) → 4,6-dimethoxy-2-aminopyrimidine (36315-01-2,256642-28-1) + N,N-dimethyl-2-(aminosulfonyl)-3-pyridinecarboxamide (112006-75-4)

Guidance literature:

With disodium hydrogenphosphate; citric acid; at 30 ℃; pH=4; Further Variations:; pH-values; Kinetics;

DOI:10.1021/jf010873s

Reference yield: 95.7%

4,6-dimethoxy-2-aminopyrimidine (36315-01-2,256642-28-1) + 2-(2,2-difluoroethoxy)-6-(trifluoromethyl)phenylsulfonamidocarboxylic acid ethyl ester → C16H15F5N4O6S

Guidance literature:

In toluene; at 100 ℃; for 6h;

Reference yield: 94.0%

4,6-dimethoxy-2-aminopyrimidine (36315-01-2,256642-28-1) + C10H8INO6S → sodium ((4,6-dimethoxypyrimidin-2-yl)carbamoyl)((2-((2-iodoethoxy)carbonyl)phenoxy)sulfonyl)amide

Guidance literature:

4,6-dimethoxy-2-aminopyrimidine; C₁₀H₈INO₆S; In acetonitrile; at 20 ℃; for 24h;

With sodium hydrogencarbonate;

DOI:10.1016/j.ejmech.2018.11.005

upstream raw materials:

nicosulfuron

Downstream raw materials:

N-<(4,6-Dimethoxypyrimidin-2-ylamino)-2,2,2-trichlorethyl>toluol-2-sulfonsaeureamid

N-<(4,6-Dimethoxypyrimidin-2-ylamino)-2,2,2-trichlorethyl>-2-chlorbenzolsaeureamid

N-<(4,6-Dimethoxypyrimidin-2-ylamino)-2,2,2-trichlorethyl>-2,6-dichlorbenzolsaeureamid

2-chloro-N-(4,6-dimethoxy-pyrimidin-2-yl)acetamide

Refernces