trans-4-Propylcyclohexanemethanol

Base Information

• Chemical Name: trans-4-Propylcyclohexanemethanol
• CAS No.: 71458-06-5
• Molecular Formula: C10H20O
• Molecular Weight: 156.268
• Hs Code.: 2906199090
• Mol file: 71458-06-5.mol

Synonyms:4-Propyl-trans- Cyclohexanemethanol;

Chemical Property of trans-4-Propylcyclohexanemethanol

Chemical Property:

• Boiling Point: 222.517 °C at 760 mmHg
• PKA: 15.05±0.10(Predicted)
• Flash Point: 96.45 °C
• PSA: 20.23000
• Density: 0.873 g/cm³
• LogP: 2.58520

Purity/Quality:

99%, ^*data from raw suppliers

(trans-4-Propylcyclohexyl)methanol 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of trans-4-Propylcyclohexanemethanol

There total 10 articles about trans-4-Propylcyclohexanemethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

trans-4-propyl-cyclohexanecarboxylic acid (38289-27-9) → trans-4-propyl-1-(hydroxymethyl)cyclohexane (71458-06-5)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether; at 0 - 20 ℃; for 1h; Inert atmosphere;

Reference yield: 91.0%

trans-4-propylcyclohexanecarbonyl chloride (67589-88-2) → trans-4-propyl-1-(hydroxymethyl)cyclohexane (71458-06-5)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether;

Reference yield:

trans,trans-4,4'-dipropyl cyclohexyl cyclohexanoate → propylcyclohexane (1678-92-8) + trans-4-propyl-1-(hydroxymethyl)cyclohexane (71458-06-5) + all-trans-4-[[(4-propylcyclohexyl)oxy]methyl]-4-propyl-cyclohexane

Guidance literature:

With di-tert-butyl peroxide; trichlorosilane; In tetrahydrofuran; at 20 ℃; for 4h; UV-irradiation;

upstream raw materials:

trans-4-propyl-cyclohexanecarboxylic acid

trans-4-propylcyclohexanecarbonyl chloride

trans-4-cyclohexanol

trans-4-n-propyl-1-bromomethylcyclohexane

Downstream raw materials:

trans-4-propyl-1-(cyanomethyl)cyclohexane

C₁₀H₁₉BrMg

1-(4'-Bromo-biphenyl-4-yl)-2-(4-propyl-cyclohexyl)-ethanone

1-(4'-Chloro-biphenyl-4-yl)-2-(4-propyl-cyclohexyl)-ethanone

Refernces

• 1、 -. "Process for the preparation of liquid crystalline ethers". Page/Page column 8-11. . Retrieved 2010/02/11.
• 2、 Carr, N.,Gray, G. W.. "The Properties of Liquid Crystal Materials Incorporating the -CH2O- Inter-ring Linkage". . p. 27 - 44. Retrieved 2007/10/02.