(NC₅H₃(C(CH₃)NC₆H₃Cl₂)2)Ir(OCH₃)

Base Information

Chemical Name:(NC₅H₃(C(CH₃)NC₆H₃Cl₂)2)Ir(OCH₃)
CAS No.:1332882-71-9
Molecular Formula:C₂₂H₁₈Cl₄IrN₃O
Molecular Weight:674.436
Hs Code.:

(NC<sub>5</sub>H<sub>3</sub>(C(CH<sub>3</sub>)NC<sub>6</sub>H<sub>3</sub>Cl<sub>2</sub>)2)Ir(OCH<sub>3</sub>)

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Chemical Property of (NC₅H₃(C(CH₃)NC₆H₃Cl₂)2)Ir(OCH₃)

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Technology Process of (NC₅H₃(C(CH₃)NC₆H₃Cl₂)2)Ir(OCH₃)

There total 2 articles about (NC₅H₃(C(CH₃)NC₆H₃Cl₂)2)Ir(OCH₃) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1332882-70-8
(NC₅H₃(C(CH₃)NC₆H₃Cl₂)2)IrCl

: 124-41-4
sodium methylate

: 1332882-71-9
(NC₅H₃(C(CH₃)NC₆H₃Cl₂)2)Ir(OCH₃)

Guidance literature:: In tetrahydrofuran; methanol; (N2) suspn. Ir complex and MeONa in MeOH-THF was stirred for 16 h; solvents were removed in vacuo, residual solvents were co-evaporated with pentane, dried in vacuo and extd. into toluene, soln. was evapd.; elem. anal.;
DOI:10.1039/c1dt10886g

Reference yield:

: 323179-70-0
2,6-bis[1-(2,6-dichlorophenylimino)ethyl]pyridine

: 1332882-71-9
(NC₅H₃(C(CH₃)NC₆H₃Cl₂)2)Ir(OCH₃)

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran; diethyl ether

2: tetrahydrofuran; methanol

In tetrahydrofuran; methanol; diethyl ether;
DOI:10.1039/c1dt10886g

Reference yield: 91.0%

: 4648-54-8
trimethylsilylazide

: 1332882-71-9
(NC₅H₃(C(CH₃)NC₆H₃Cl₂)2)Ir(OCH₃)

: 1332882-75-3
(NC₅H₃(C(CH₃)NC₆H₃Cl₂)2)IrN₃

Guidance literature:: In tetrahydrofuran; (N2) to soln. Ir complex in THF at -35°C soln. Me3SiN3 in THF wasadded and stored atv -35°C for 2.5 h; solvent was removed in vacuo, residual solvent was co-evapd. with pentane and dried in vacuo for 4 h;
DOI:10.1039/c1dt10886g