C₄₅H₄₆O₈

Base Information

• Chemical Name: C₄₅H₄₆O₈
• CAS No.: 1225283-71-5
• Molecular Formula: C₄₅H₄₆O₈
• Molecular Weight: 714.855
• Mol file: 1225283-71-5.mol

Synonyms:

Chemical Property of C₄₅H₄₆O₈

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₅H₄₆O₈

There total 7 articles about C₄₅H₄₆O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C52H52O8 → C45H46O8 (1225283-71-5)

Guidance literature:

With 20 % Pd(OH)2/C; hydrogen; In ethyl acetate; at 20 ℃;

DOI:10.1021/cm100134f

Reference yield:

3-Bromophenol (591-20-8) → C45H46O8 (1225283-71-5)

Guidance literature:

Multi-step reaction with 5 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / 1,2-dimethoxyethane; water / 15 h / Reflux

2: dmap; dicyclohexyl-carbodiimide / chloroform / 20 °C

3: 20 % Pd(OH)2/C; hydrogen / ethyl acetate / 20 °C

4: dmap; dicyclohexyl-carbodiimide / chloroform / 20 °C

5: 20 % Pd(OH)2/C; hydrogen / ethyl acetate / 20 °C

With dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 20 % Pd(OH)2/C; hydrogen; sodium carbonate; dicyclohexyl-carbodiimide; In 1,2-dimethoxyethane; chloroform; water; ethyl acetate;

DOI:10.1021/cm100134f

Reference yield:

[4-(benzyloxy)phenyl]boronic acid (146631-00-7) → C45H46O8 (1225283-71-5)

Guidance literature:

Multi-step reaction with 5 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / 1,2-dimethoxyethane; water / 15 h / Reflux

2: dmap; dicyclohexyl-carbodiimide / chloroform / 20 °C

3: 20 % Pd(OH)2/C; hydrogen / ethyl acetate / 20 °C

4: dmap; dicyclohexyl-carbodiimide / chloroform / 20 °C

5: 20 % Pd(OH)2/C; hydrogen / ethyl acetate / 20 °C

With dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 20 % Pd(OH)2/C; hydrogen; sodium carbonate; dicyclohexyl-carbodiimide; In 1,2-dimethoxyethane; chloroform; water; ethyl acetate;

DOI:10.1021/cm100134f

upstream raw materials:

3-Bromophenol

[4-(benzyloxy)phenyl]boronic acid

4-(4-dodecyloxybenzoyloxy)benzoic acid

4'-(benzyloxy)-1,1'-biphenyl-3-ol

Downstream raw materials:

C₇₂H₉₆O₁₀Si₃

C₆₉H₈₈O₁₀Si₂

C₆₆H₈₀O₁₀Si

C₇₂H₉₆O₁₀Si₃

Refernces