Benzoic acid, 4-(dodecyloxy)-, 4-carboxyphenyl ester

Base Information

• Chemical Name: Benzoic acid, 4-(dodecyloxy)-, 4-carboxyphenyl ester
• CAS No.: 106817-35-0
• Molecular Formula: C26H34O5
• Molecular Weight: 426.553
• Mol file: 106817-35-0.mol

Synonyms:

Chemical Property of Benzoic acid, 4-(dodecyloxy)-, 4-carboxyphenyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzoic acid, 4-(dodecyloxy)-, 4-carboxyphenyl ester

There total 22 articles about Benzoic acid, 4-(dodecyloxy)-, 4-carboxyphenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

4-formylphenyl 4-(dodecyloxy)benzoate (56800-36-3) → 4-(4-dodecyloxybenzoyloxy)benzoic acid (106817-35-0)

Guidance literature:

With sodium chlorite; sodium dihydrogen phosphate monohydrate; recorcinol; In water; tert-butyl alcohol; at 20 ℃; Inert atmosphere;

DOI:10.1039/b802554a

Reference yield: 98.0%

4-[(benzyloxy)carbonyl]phenyl 4-dodecyloxybenzoate (412943-62-5) → 4-(4-dodecyloxybenzoyloxy)benzoic acid (106817-35-0)

Guidance literature:

With 20 % Pd(OH)2/C; hydrogen; In tetrahydrofuran; for 7h; under 45004.5 Torr;

DOI:10.1039/c0jm04570e

Reference yield:

Benzyl 4-hydroxybenzoate (94-18-8) → 4-(4-dodecyloxybenzoyloxy)benzoic acid (106817-35-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 4-(N,N-dimethylamino)pyridine; N,N'-dicyclohexylcarbodiimide / CH₂Cl₂ / 20 °C

2: cyclohexene; ethanol / Pd(OH)2/C / 8 h / Heating

With dmap; ethanol; dicyclohexyl-carbodiimide; cyclohexene; palladium dihydroxide; In dichloromethane;

DOI:10.1021/ja0585477

upstream raw materials:

4-dodecyloxybenzoyl chloride

4-hydroxy-benzoic acid

4-formylphenyl 4-(dodecyloxy)benzoate

4-[(benzyloxy)carbonyl]phenyl 4-dodecyloxybenzoate

Downstream raw materials:

CH₃C(O)CH(OC(O)C₆H₄OC(O)C₆H₄O(CH₂)11CH₃)C(O)CH₃

4-((3-(4-(4-(12-bromododecyloxy)benzoyloxy)benzoyloxy)phenoxy)carbonyl)phenyl 4-(dodecyloxy)benzoate

4,4'-dodecyloxybenzoyloxybenzoyl-4-oxy-2-hydroxybenzaldehyde

3-[4-(4-n-dodecyloxybenzoyloxy)-2-hydroxybenzylideneamino]-6-methylphenyl 4-(4-n-dodecyloxybenzoyloxy)benzoate