C₂₁H₃₁ClSi

Base Information

Chemical Name:C₂₁H₃₁ClSi
CAS No.:1453803-62-7
Molecular Formula:C₂₁H₃₁ClSi
Molecular Weight:347.016
Hs Code.:

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Chemical Property of C₂₁H₃₁ClSi

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Technology Process of C₂₁H₃₁ClSi

There total 2 articles about C₂₁H₃₁ClSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1037048-15-9
1-(buta-2,3-dien-2-yl)-4-chlorobenzene

: 89343-06-6
tris-iso-propylsilyl acetylene

: 1453803-52-5
C₂₁H₃₁ClSi

: 1453803-62-7
C₂₁H₃₁ClSi

Guidance literature:: With cobalt(II) acetate tetrahydrate; C₅₄H₈₀FeO₂P₂; zinc; In dimethyl sulfoxide; at 80 ℃; for 3h; Overall yield = 81 %; Overall yield = 56.4 mg; enantioselective reaction; Inert atmosphere;
DOI:10.1021/jo401604n

Reference yield:

: 1064000-89-0
1-chloro-4-(2,2-dibromo-1-methylcyclopropyl)benzene

: 1453803-52-5
C₂₁H₃₁ClSi

: 1453803-62-7
C₂₁H₃₁ClSi

Guidance literature:: Multi-step reaction with 2 steps

1: methyllithium / diethyl ether / 1.5 h / -40 °C / Inert atmosphere

2: zinc; C₅₄H₈₀FeO₂P₂; cobalt(II) acetate tetrahydrate / dimethyl sulfoxide / 3 h / 80 °C / Inert atmosphere

With cobalt(II) acetate tetrahydrate; C₅₄H₈₀FeO₂P₂; methyllithium; zinc; In diethyl ether; dimethyl sulfoxide;
DOI:10.1021/jo401604n