C₂₅H₂₃ClF₃N₇O₂

Base Information

Chemical Name:C₂₅H₂₃ClF₃N₇O₂
CAS No.:1620069-03-5
Molecular Formula:C₂₅H₂₃ClF₃N₇O₂
Molecular Weight:545.952
Hs Code.:

C<sub>25</sub>H<sub>23</sub>ClF<sub>3</sub>N<sub>7</sub>O<sub>2</sub>

Synonyms:

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Chemical Property of C₂₅H₂₃ClF₃N₇O₂

Chemical Property:

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Technology Process of C₂₅H₂₃ClF₃N₇O₂

There total 8 articles about C₂₅H₂₃ClF₃N₇O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: ethyl 2-(3-nitrophenyl)acetimidate

: 1620069-03-5
C₂₅H₂₃ClF₃N₇O₂

Guidance literature:: Multi-step reaction with 7 steps

1: ethanol / 4 h / 40 °C

2: hydrogenchloride / water; methanol / 1 h / 90 °C

3: palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; potassium phosphate / toluene / 130 °C

4: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 20 °C

5: tetrahydrofuran / 6 h / 60 °C

6: hydrogen / methanol

7: tetrahydrofuran / 20 °C

With hydrogenchloride; potassium phosphate; hydrogen; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; toluene; 3: |Buchwald-Hartwig Coupling;
DOI:10.1016/j.bmcl.2014.05.030

Reference yield:

: 621-50-1
(3-nitrophenyl)acetonitrile

: 1620069-03-5
C₂₅H₂₃ClF₃N₇O₂

Guidance literature:: Multi-step reaction with 8 steps

1: hydrogenchloride / 3 h / -10 °C

2: ethanol / 4 h / 40 °C

3: hydrogenchloride / water; methanol / 1 h / 90 °C

4: palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; potassium phosphate / toluene / 130 °C

5: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 20 °C

6: tetrahydrofuran / 6 h / 60 °C

7: hydrogen / methanol

8: tetrahydrofuran / 20 °C

With hydrogenchloride; potassium phosphate; hydrogen; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; toluene; 4: |Buchwald-Hartwig Coupling;
DOI:10.1016/j.bmcl.2014.05.030

Reference yield:

: 1620069-18-2
N-(2,2-dimethoxyethyl)-2-(3-nitrophenyl)acetimidamide

: 1620069-03-5
C₂₅H₂₃ClF₃N₇O₂

Guidance literature:: Multi-step reaction with 6 steps

1: hydrogenchloride / water; methanol / 1 h / 90 °C

2: palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; potassium phosphate / toluene / 130 °C

3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 20 °C

4: tetrahydrofuran / 6 h / 60 °C

5: hydrogen / methanol

6: tetrahydrofuran / 20 °C

With hydrogenchloride; potassium phosphate; hydrogen; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; dichloromethane; water; toluene; 2: |Buchwald-Hartwig Coupling;
DOI:10.1016/j.bmcl.2014.05.030