Cyclohexyl(phenyl)methanamine

Base Information

• Chemical Name: Cyclohexyl(phenyl)methanamine
• CAS No.: 23459-35-0
• Molecular Formula: C13H19N
• Molecular Weight: 189.301
• Hs Code.: 2921499090
• DSSTox Substance ID: DTXSID30453904
• Nikkaji Number: J1.156.103I
• Mol file: 23459-35-0.mol

Synonyms:cyclohexyl(phenyl)methanamine;23459-35-0;starbld0018340;alpha-Cyclohexylbenzylamine;a-Cyclohexylbenzenemethanamine;SCHEMBL182619;c-cyclohexyl-c-phenyl-methylamine;DTXSID30453904;JQCBKIHKSZUZKT-UHFFFAOYSA-N;AKOS000199756;CS-0433749;EN300-57963;F80172;AB01000446-01

Chemical Property of Cyclohexyl(phenyl)methanamine

Chemical Property:

• Vapor Pressure: 0.002mmHg at 25°C
• Boiling Point: 293.873°C at 760 mmHg
• Flash Point: 122.919°C
• PSA: 26.02000
• Density: 1.001g/cm³
• LogP: 3.96700
• XLogP3: 3.2
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 2
• Exact Mass: 189.151749610
• Heavy Atom Count: 14
• Complexity: 155

Purity/Quality:

97% ^*data from raw suppliers

1-CYCLOHEXYL-1-PHENYLMETHANAMINE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CCC(CC1)C(C2=CC=CC=C2)N

Technology Process of Cyclohexyl(phenyl)methanamine

There total 29 articles about Cyclohexyl(phenyl)methanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.1%

R-α-cyclohexylbenzyl acetamide → R-α-cyclohexylbenzylamine (23459-35-0,32908-31-9,32908-33-1,32908-36-4)

Guidance literature:

With hydrogenchloride; In methanol; Reflux;

Reference yield: 92.0%

Cyclohexyl phenyl ketone (712-50-5) → cyclohexyl(phenyl)methanamine (23459-35-0)

Guidance literature:

Cyclohexyl phenyl ketone; With ammonium acetate; In methanol; at 25 ℃; for 0.166667h;

With sodium cyanoborohydride; In methanol; at 60 ℃; for 16h;

With sodium hydroxide; In water;

DOI:10.1016/j.bmc.2014.06.027

Reference yield: 91.0%

N-[cyclohexyl(phenyl)methylidene]hydroxylamine (1136-58-9) → cyclohexyl(phenyl)methanamine (23459-35-0)

Guidance literature:

N-[cyclohexyl(phenyl)methylidene]hydroxylamine; With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 8h; Heating / reflux;

With sodium hydroxide; water; at 0 ℃;

upstream raw materials:

N-[cyclohexyl(phenyl)methylidene]hydroxylamine

(Z)-cyclohexyl(phenyl)methanone oxime

(E)-cyclohexyl(phenyl)methanone oxime

Cyclohexyl phenyl ketone

Downstream raw materials:

N-(Cyclohexylphenylmethyl)-N_.N-dimethylamin

C₂₀H₂₃NO

N-(cyclohexyl(phenyl)methyl)-3-(3-sulfamoylphenyl)-1H-indazole-5-carboxamide

(+/-)-N-(α-Cyclohexyl-benzyl)-N',N'-dimethyl-aethylendiamin