Technology Process of 6-(benzyloxy)-7,8,12-trimethoxy-3-methyl-1,2,3,4-tetrahydrotetraphene
There total 5 articles about 6-(benzyloxy)-7,8,12-trimethoxy-3-methyl-1,2,3,4-tetrahydrotetraphene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium hydroxide;
In
tetrahydrofuran; water;
at 20 ℃;
for 2.5h;
Inert atmosphere;
DOI:10.1002/cjoc.201201084
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / N,N-dimethyl-formamide / 20 °C / Inert atmosphere
2: tetrabutylammomium bromide; sodium dithionite / tetrahydrofuran; water / 0.5 h / Inert atmosphere
3: potassium hydroxide / tetrahydrofuran; water / 2.5 h / 20 °C / Inert atmosphere
With
sodium dithionite; tetrabutylammomium bromide; potassium carbonate; potassium hydroxide;
In
tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1002/cjoc.201201084
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tetrabutylammomium bromide; sodium dithionite / tetrahydrofuran; water / 0.5 h / Inert atmosphere
2: potassium hydroxide / tetrahydrofuran; water / 2.5 h / 20 °C / Inert atmosphere
With
sodium dithionite; tetrabutylammomium bromide; potassium hydroxide;
In
tetrahydrofuran; water;
DOI:10.1002/cjoc.201201084
