Co(II)(triphenylphosphine oxide)2Cl₂

Base Information

Chemical Name:Co(II)(triphenylphosphine oxide)2Cl₂
CAS No.:14494-82-7
Molecular Formula:C₃₆H₃₀Cl₂CoO₂P₂
Molecular Weight:686.48
Hs Code.:

Co(II)(triphenylphosphine oxide)2Cl<sub>2</sub>

Synonyms:

Suppliers and Price of Co(II)(triphenylphosphine oxide)2Cl₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Co(II)(triphenylphosphine oxide)2Cl₂

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Co(II)(triphenylphosphine oxide)2Cl₂

There total 3 articles about Co(II)(triphenylphosphine oxide)2Cl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.8%

: 791-28-6
Triphenylphosphine oxide

: 7646-79-9,14543-09-0,16413-89-1
cobalt(II) chloride

: 14494-82-7
Co(II)(triphenylphosphine oxide)2Cl₂

Guidance literature:: In ethanol; formation from CoCl2 and triphenylphosphine oxide in alcohol; evapn. after addn. of benzene;; washing with ether/benzene mixt.;;

Reference yield: 21.0%

: 80462-11-9
(C₆H₅)3PCo(HONC(CH₃)C(CH₃)NO)2(N₃C₂)(CO₂CH₃)2

: 75-36-5
acetyl chloride

: 80461-78-5
C₈H₉N₃O₅

: 14494-82-7
Co(II)(triphenylphosphine oxide)2Cl₂

Guidance literature:: In neat (no solvent); (CH3CO2)2(C2N3)Co(DH)2PPh3 stirred with acetyl chloride for 10 min at room temp.; oil pumped under high vac. and extd. with abs. Et2O, residue - (Ph3PO)2CoCl2;
DOI:10.1021/ic00133a069

Reference yield:

: cobalt(II) chloride hexahydrate

: 791-28-6
Triphenylphosphine oxide

: 14494-82-7
Co(II)(triphenylphosphine oxide)2Cl₂

Guidance literature:: In ethanol; addn. of hot soln. of 2 equiv. OPPh3 to hot soln. of CoCl2; crystn. on cooling (1 h), filtration, washing (Et2O), drying (vac.); elem. anal.;
DOI:10.1039/DT9950001095