1-([1-(dimethylamino)-1-methylethyl]phenyl)-3,4,4-trimethyl-1,2,3,4-tetrahydro-3,1-benzaazaborin

Base Information

• Chemical Name: 1-([1-(dimethylamino)-1-methylethyl]phenyl)-3,4,4-trimethyl-1,2,3,4-tetrahydro-3,1-benzaazaborin
• CAS No.: 258280-95-4
• Molecular Formula: C₂₂H₃₁BN₂
• Molecular Weight: 334.313
• Mol file: 258280-95-4.mol

Synonyms:

Chemical Property of 1-([1-(dimethylamino)-1-methylethyl]phenyl)-3,4,4-trimethyl-1,2,3,4-tetrahydro-3,1-benzaazaborin

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-([1-(dimethylamino)-1-methylethyl]phenyl)-3,4,4-trimethyl-1,2,3,4-tetrahydro-3,1-benzaazaborin

There total 1 articles about 1-([1-(dimethylamino)-1-methylethyl]phenyl)-3,4,4-trimethyl-1,2,3,4-tetrahydro-3,1-benzaazaborin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

Triisopropyl borate (5419-55-6) + 2-[1-(dimethylamino)-1-methylethyl]phenyllithium → 2-[1-(dimethylamino)-1-methylethyl]phenylboronic acid + 1-([1-(dimethylamino)-1-methylethyl]phenyl)-3,4,4-trimethyl-1,2,3,4-tetrahydro-3,1-benzaazaborin (258280-95-4) + [1-(dimethylamino)-1-methylethyl]benzene (938-04-5)

Guidance literature:

In diethyl ether; stirred for 15 h at room temp.; volatiles was removed in vac., ppt. was treated with CH2Cl2, filtered, evapd., treated with hexane-CH2Cl2;

DOI:10.1021/om990724n

upstream raw materials:

Triisopropyl borate

Refernces