1-(1-Iminobenzyl)-2,3-dimethylnaphthalin

Base Information

• Chemical Name: 1-(1-Iminobenzyl)-2,3-dimethylnaphthalin
• CAS No.: 19930-50-8
• Molecular Formula: C₁₉H₁₇N
• Molecular Weight: 259.351
• Mol file: 19930-50-8.mol

Synonyms:

Chemical Property of 1-(1-Iminobenzyl)-2,3-dimethylnaphthalin

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-(1-Iminobenzyl)-2,3-dimethylnaphthalin

There total 3 articles about 1-(1-Iminobenzyl)-2,3-dimethylnaphthalin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,3-dimethylnaphthalene (581-40-8) → 1-(1-Iminobenzyl)-2,3-dimethylnaphthalin (19930-50-8)

Guidance literature:

Multi-step reaction with 3 steps

1: Br₂ / CHCl₃; CCl₄

2: pyridine / 190 - 210 °C

3: (i) Et₂O, benzene, (ii) aq. NH₄Cl

With bromine; In pyridine; tetrachloromethane; chloroform;

DOI:10.1039/j39680002502

Reference yield:

1-bromo-2,3-dimethylnaphthalene (5334-79-2) → 1-(1-Iminobenzyl)-2,3-dimethylnaphthalin (19930-50-8)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / 190 - 210 °C

2: (i) Et₂O, benzene, (ii) aq. NH₄Cl

In pyridine;

DOI:10.1039/j39680002502

Reference yield:

2,3-dimethyl-1-naphthonitrile (19930-47-3) + phenylmagnesium iodide (16002-63-4) → 1-(1-Iminobenzyl)-2,3-dimethylnaphthalin (19930-50-8)

Guidance literature:

Multistep reaction; (i) Et₂O, benzene, (ii) aq. NH₄Cl;

DOI:10.1039/j39680002502

upstream raw materials:

2,3-dimethyl-1-naphthonitrile

phenylmagnesium iodide

2,3-dimethylnaphthalene

1-bromo-2,3-dimethylnaphthalene

Downstream raw materials:

(2,3-dimethylnaphthalen-1-yl)(phenyl)methanone