iron(III) octaethyltetraphenylporphyrin bis(4-cyanopyridine) perchlorate

Base Information

Chemical Name:iron(III) octaethyltetraphenylporphyrin bis(4-cyanopyridine) perchlorate
CAS No.:362651-58-9
Molecular Formula:C₇₂H₆₈FeN₈*ClO₄
Molecular Weight:1200.68
Hs Code.:

Synonyms:

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Chemical Property of iron(III) octaethyltetraphenylporphyrin bis(4-cyanopyridine) perchlorate

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Technology Process of iron(III) octaethyltetraphenylporphyrin bis(4-cyanopyridine) perchlorate

There total 3 articles about iron(III) octaethyltetraphenylporphyrin bis(4-cyanopyridine) perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 146343-96-6,953387-00-3
(2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetraphenylporphyrinate)FeCl

: 362651-58-9
iron(III) octaethyltetraphenylporphyrin bis(4-cyanopyridine) perchlorate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran

2: dichloromethane

In tetrahydrofuran; dichloromethane;
DOI:10.1002/1521-3773(20010716)40:14<2617::AID-ANIE2617>3.0.CO;2-B

Reference yield:

: 100-48-1
pyridine-4-carbonitrile

: [(2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetraphenylporphyrin)(C₄H₄O)2Fe]ClO₄

: 362651-58-9
iron(III) octaethyltetraphenylporphyrin bis(4-cyanopyridine) perchlorate

Guidance literature:: In dichloromethane; soln. Fe(oetpp)(THF)2ClO4 (CH2Cl2); excess of ligand (4-CNpy) added; recrystn. (CH2Cl2/heptane);
DOI:10.1002/1521-3773(20010716)40:14<2617::AID-ANIE2617>3.0.CO;2-B

Reference yield:

: 100-48-1
pyridine-4-carbonitrile

: 343849-31-0
(2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetraphenylporphyrinato)iron(III) perchlorate

: 362651-58-9
iron(III) octaethyltetraphenylporphyrin bis(4-cyanopyridine) perchlorate

Guidance literature:: In dichloromethane-d2; a soln. of Fe complex added to ligand, heated for 5 min, more ligand added; not isolated, detected by NMR;
DOI:10.1021/ic035010q