[iron(III)(2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetraphenylporphyrin)(ClO₄)]

Base Information

• Chemical Name: [iron(III)(2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetraphenylporphyrin)(ClO₄)]
• CAS No.: 343849-31-0
• Molecular Formula: C₆₀H₆₀ClFeN₄O₄
• Molecular Weight: 992.461

Synonyms:

Chemical Property of [iron(III)(2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetraphenylporphyrin)(ClO₄)]

Chemical Property:

Purity/Quality:

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Useful:

Technology Process of [iron(III)(2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetraphenylporphyrin)(ClO₄)]

There total 2 articles about [iron(III)(2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetraphenylporphyrin)(ClO₄)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetraphenylporphyrinate)FeCl (146343-96-6,953387-00-3) + silver perchlorate → (2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetraphenylporphyrinato)iron(III) perchlorate (343849-31-0)

Guidance literature:

In tetrahydrofuran; Fe complex dissolved in THF, heated, AgClO4 in THF added, refluxed; cooled to room temp., filtered, toluene added, evapd. (vac., 50°C), dissolved in boiling toluene, boiling heptane added, crystd., filtered, washed (cold heptane), dried (vac., 60°C); obtained as contg. toluene;

DOI:10.1021/ic035010q

Reference yield:

(chloro)(2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetrphenylporphyrinato)iron(III) complex (953387-00-3,146343-96-6) + silver perchlorate → (2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetraphenylporphyrinato)iron(III) perchlorate (343849-31-0)

Guidance literature:

In tetrahydrofuran; 1.0 equiv. AgClO4; recrystd. from THF-hexane;

DOI:10.1246/cl.2000.342

Reference yield:

1-methyl-1H-imidazole (616-47-7) + [iron(III)(2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetraphenylporphyrin)(ClO4)] (343849-31-0) + nitrogen(II) oxide (10102-43-9) + chlorobenzene (108-90-7) → [Fe(octaethyltetraphenylporphyrin)(1-methylimidazole)(NO)](ClO4)*chlorobenzene

Guidance literature:

In chlorobenzene; C6H5Cl was added to Fe-complex and soln. of ligand in C6H5Cl under Ar, NO was bubbled into soln. for several min; hexane was layered over soln.;

DOI:10.1021/ja0207145

upstream raw materials:

(2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetraphenylporphyrinate)FeCl

(chloro)(2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetrphenylporphyrinato)iron(III) complex

Downstream raw materials:

bis(4-dimethylaminopyridine)(2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetraphenylporphyrinato)iron(III) perchlorate

iron(III) octaethyltetraphenylporphyrin bis(4-cyanopyridine) perchlorate

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