pentaphenylcyclopentadienyltrichlorozirconium(IV)

Base Information

Chemical Name:pentaphenylcyclopentadienyltrichlorozirconium(IV)
CAS No.:241492-60-4
Molecular Formula:C₃₅H₂₅Cl₃Zr
Molecular Weight:643.167
Hs Code.:

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Chemical Property of pentaphenylcyclopentadienyltrichlorozirconium(IV)

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Technology Process of pentaphenylcyclopentadienyltrichlorozirconium(IV)

There total 1 articles about pentaphenylcyclopentadienyltrichlorozirconium(IV) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.4%

: 10026-11-6
zirconium(IV) chloride

: 82207-55-4
(pentaphenylcyclopentadienyl)lithium

: 241492-60-4
pentaphenylcyclopentadienyltrichlorozirconium(IV)

Guidance literature:: In xylene; Li-salt and ZrCl4 were mixed in xylene for 24 h; solvent was removed in vacuo, extd. with xylene for 24 h, solvent was removed in vacuo, extd. for 24 h, cooled; elem. anal.;
DOI:10.1016/S0022-328X(03)00637-5

Reference yield: 95.1%

: 241492-60-4
pentaphenylcyclopentadienyltrichlorozirconium(IV)

: lithium cyclopentadienide

: 241492-62-6
cyclopentadienyl(pentaphenylcyclopentadienyl)dichlorozirconium(IV)

Guidance literature:: In dichloromethane; Zr-complex and Li-salt were stirred in CH2Cl2 for 24 h at room temp.; solvent was removed in vacuo, extd. with CH2Cl2, cooled; elem. anal.;
DOI:10.1016/S0022-328X(03)00637-5