Technology Process of C27H20O
There total 7 articles about C27H20O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: tert-butyllithium (t-BuLi) / tetrahydrofuran; pentane / 0.75 h / -78 °C
2: 1,2-dibromoethane / Ambient temperature
3: 66 percent / acetophenone / diethyl ether / Ambient temperature; Irradiation
With
tert.-butyl lithium; ethylene dibromide; acetophenone;
In
tetrahydrofuran; diethyl ether; pentane;
DOI:10.1021/ja00172a031
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 34 percent / 4-toluenesulfonyl chloride
2: tert-butyllithium (t-BuLi) / tetrahydrofuran; pentane / 0.75 h / -78 °C
3: 1,2-dibromoethane / Ambient temperature
4: 66 percent / acetophenone / diethyl ether / Ambient temperature; Irradiation
With
tert.-butyl lithium; ethylene dibromide; acetophenone; p-toluenesulfonyl chloride;
In
tetrahydrofuran; diethyl ether; pentane;
DOI:10.1021/ja00172a031
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1,2-dibromoethane / Ambient temperature
2: 66 percent / acetophenone / diethyl ether / Ambient temperature; Irradiation
With
ethylene dibromide; acetophenone;
In
diethyl ether;
DOI:10.1021/ja00172a031
