Technology Process of C15H16N4O2
There total 5 articles about C15H16N4O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: N,N,N,N,N,N-hexamethylphosphoric triamide; sodium hydride / tetrahydrofuran
2: potassium tert-butylate / tert-butyl alcohol
With
N,N,N,N,N,N-hexamethylphosphoric triamide; potassium tert-butylate; sodium hydride;
In
tetrahydrofuran; tert-butyl alcohol;
1: Baker-Venkataraman transformation;
DOI:10.1016/j.bmcl.2011.05.081
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethylamine / tetrahydrofuran
2: N,N,N,N,N,N-hexamethylphosphoric triamide; sodium hydride / tetrahydrofuran
3: potassium tert-butylate / tert-butyl alcohol
With
N,N,N,N,N,N-hexamethylphosphoric triamide; potassium tert-butylate; sodium hydride; triethylamine;
In
tetrahydrofuran; tert-butyl alcohol;
2: Baker-Venkataraman transformation;
DOI:10.1016/j.bmcl.2011.05.081
- Guidance literature:
-
Multi-step reaction with 4 steps
1: carbon disulfide; aluminum (III) chloride / acetonitrile
2: triethylamine / tetrahydrofuran
3: N,N,N,N,N,N-hexamethylphosphoric triamide; sodium hydride / tetrahydrofuran
4: potassium tert-butylate / tert-butyl alcohol
With
carbon disulfide; N,N,N,N,N,N-hexamethylphosphoric triamide; aluminum (III) chloride; potassium tert-butylate; sodium hydride; triethylamine;
In
tetrahydrofuran; acetonitrile; tert-butyl alcohol;
1: Fries rearrangement / 3: Baker-Venkataraman transformation;
DOI:10.1016/j.bmcl.2011.05.081
