Technology Process of C22H28N2O12S2
There total 6 articles about C22H28N2O12S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: sodium hydride / N,N-dimethyl-formamide
2: water; acetic acid
3: sodium periodate
4: sodium hydroxide
6: sulfuric acid; acetic acid
7: trimethylsilyl trifluoromethanesulfonate; BSA
With
sodium periodate; trimethylsilyl trifluoromethanesulfonate; sulfuric acid; water; sodium hydride; acetic acid; sodium hydroxide; BSA;
In
N,N-dimethyl-formamide;
7: Vorbruggen reaction;
DOI:10.1016/j.bmcl.2011.06.104
- Guidance literature:
-
Multi-step reaction with 8 steps
1: lithium triethylborohydride / dichloromethane
2: sodium hydride / N,N-dimethyl-formamide
3: water; acetic acid
4: sodium periodate
5: sodium hydroxide
7: sulfuric acid; acetic acid
8: trimethylsilyl trifluoromethanesulfonate; BSA
With
sodium periodate; trimethylsilyl trifluoromethanesulfonate; sulfuric acid; water; sodium hydride; lithium triethylborohydride; acetic acid; sodium hydroxide; BSA;
In
dichloromethane; N,N-dimethyl-formamide;
8: Vorbruggen reaction;
DOI:10.1016/j.bmcl.2011.06.104
- Guidance literature:
-
Multi-step reaction with 6 steps
1: water; acetic acid
2: sodium periodate
3: sodium hydroxide
5: sulfuric acid; acetic acid
6: trimethylsilyl trifluoromethanesulfonate; BSA
With
sodium periodate; trimethylsilyl trifluoromethanesulfonate; sulfuric acid; water; acetic acid; sodium hydroxide; BSA;
6: Vorbruggen reaction;
DOI:10.1016/j.bmcl.2011.06.104