1-<1-<2-<(3-chloro-5-hydroxybenzyl)oxy>phenyl>vinyl>-1H-imidazole hydrochloride

Base Information

Chemical Name:1-<1-<2-<(3-chloro-5-hydroxybenzyl)oxy>phenyl>vinyl>-1H-imidazole hydrochloride
CAS No.:98406-10-1
Molecular Formula:C₁₈H₁₅ClN₂O₂*ClH
Molecular Weight:363.243
Hs Code.:

Synonyms:

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Chemical Property of 1-<1-<2-<(3-chloro-5-hydroxybenzyl)oxy>phenyl>vinyl>-1H-imidazole hydrochloride

Chemical Property:

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Technology Process of 1-<1-<2-<(3-chloro-5-hydroxybenzyl)oxy>phenyl>vinyl>-1H-imidazole hydrochloride

There total 10 articles about 1-<1-<2-<(3-chloro-5-hydroxybenzyl)oxy>phenyl>vinyl>-1H-imidazole hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 98406-08-7
1-<1-<2-<(3-chloro-5-methoxymethyloxybenzyl)oxy>phenyl>vinyl>-1H-imidazole

: 98406-10-1
1-<1-<2-<(3-chloro-5-hydroxybenzyl)oxy>phenyl>vinyl>-1H-imidazole hydrochloride

Guidance literature:: With hydrogenchloride; In methanol; dichloromethane; ethyl acetate; for 2h; Ambient temperature;

Reference yield:

: 51-36-5
3,5-dichlorobenzoic acid

: 98406-10-1
1-<1-<2-<(3-chloro-5-hydroxybenzyl)oxy>phenyl>vinyl>-1H-imidazole hydrochloride

Guidance literature:: Multi-step reaction with 8 steps

1: hexamethylphosphoramide / 15 h / 115 - 120 °C

2: 70 percent / acetyl chloride / 15 h / Ambient temperature

3: 93 percent / BBr₃ / CH₂Cl₂ / 3 h / 0 °C

4: 93 percent / NaH / tetrahydrofuran / 3 h / Ambient temperature

5: 70 percent / LiAlH₄ / tetrahydrofuran / 0.5 h / Ambient temperature

6: 29 percent / SOCl₂ / benzene / 0.5 h / Heating

7: 64 percent / NaH / dimethylformamide / 15 h / Ambient temperature

8: 61 percent / 10percent HCl / ethyl acetate; CH₂Cl₂; methanol / 2 h / Ambient temperature

With hydrogenchloride; N,N,N,N,N,N-hexamethylphosphoric triamide; lithium aluminium tetrahydride; thionyl chloride; boron tribromide; sodium hydride; acetyl chloride; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; benzene;

Reference yield:

: 82477-67-6
3-chloro-5-methoxy-benzoic acid

: 98406-10-1
1-<1-<2-<(3-chloro-5-hydroxybenzyl)oxy>phenyl>vinyl>-1H-imidazole hydrochloride

Guidance literature:: Multi-step reaction with 7 steps

1: 70 percent / acetyl chloride / 15 h / Ambient temperature

2: 93 percent / BBr₃ / CH₂Cl₂ / 3 h / 0 °C

3: 93 percent / NaH / tetrahydrofuran / 3 h / Ambient temperature

4: 70 percent / LiAlH₄ / tetrahydrofuran / 0.5 h / Ambient temperature

5: 29 percent / SOCl₂ / benzene / 0.5 h / Heating

6: 64 percent / NaH / dimethylformamide / 15 h / Ambient temperature

7: 61 percent / 10percent HCl / ethyl acetate; CH₂Cl₂; methanol / 2 h / Ambient temperature

With hydrogenchloride; lithium aluminium tetrahydride; thionyl chloride; boron tribromide; sodium hydride; acetyl chloride; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; benzene;