C₂₄H₂₁ClN₄O₂

Base Information

Chemical Name:C₂₄H₂₁ClN₄O₂
CAS No.:1357089-46-3
Molecular Formula:C₂₄H₂₁ClN₄O₂
Molecular Weight:432.909
Hs Code.:

C<sub>24</sub>H<sub>21</sub>ClN<sub>4</sub>O<sub>2</sub>

Synonyms:

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Chemical Property of C₂₄H₂₁ClN₄O₂

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Technology Process of C₂₄H₂₁ClN₄O₂

There total 7 articles about C₂₄H₂₁ClN₄O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 1357089-67-8
C₂₀H₁₄ClN₃O₂

: 43204-63-3
bis(2-bromoethyl)amine hydrobromide

: 1357089-46-3
C₂₄H₂₁ClN₄O₂

Guidance literature:: With aluminum oxide; at 120 ℃; for 12h;
DOI:10.1016/j.bmcl.2011.11.113

Reference yield:

: 175276-64-9
5-(4-chlorophenyl)-2-formylfuran-3-carboxylic acid ethyl ester

: 1357089-46-3
C₂₄H₂₁ClN₄O₂

Guidance literature:: Multi-step reaction with 7 steps

1: N-Bromosuccinimide / dichloromethane / 12 h

2: [bis(acetoxy)iodo]benzene; potassium carbonate / dimethyl sulfoxide / 12 h

3: diisobutylaluminium hydride / tetrahydrofuran / -78 °C

4: caesium carbonate / N,N-dimethyl-formamide / 12 h / 65 °C

5: potassium tert-butylate / tetrahydrofuran / 6 h

6: acetic acid; zinc / 2 h

7: aluminum oxide / 12 h / 120 °C

With aluminum oxide; N-Bromosuccinimide; [bis(acetoxy)iodo]benzene; potassium tert-butylate; diisobutylaluminium hydride; potassium carbonate; caesium carbonate; acetic acid; zinc; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.11.113

Reference yield:

: 1357089-58-7
C₁₄H₁₁ClN₂O₂

: 1357089-46-3
C₂₄H₂₁ClN₄O₂

Guidance literature:: Multi-step reaction with 4 steps

1: caesium carbonate / N,N-dimethyl-formamide / 12 h / 65 °C

2: potassium tert-butylate / tetrahydrofuran / 6 h

3: acetic acid; zinc / 2 h

4: aluminum oxide / 12 h / 120 °C

With aluminum oxide; potassium tert-butylate; caesium carbonate; acetic acid; zinc; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.11.113