Technology Process of C15H17(2)H2ClSe
There total 6 articles about C15H17(2)H2ClSe which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate; hydrazine hydrate;
In
diethylene glycol;
1) 150 deg C 2) 200 deg C;
DOI:10.1021/jo00006a006
- Guidance literature:
-
Multi-step reaction with 6 steps
1: LiAlD4 / diethyl ether
2: Et3N / diethyl ether / 25 °C
3: NaBH4 / ethanol / Heating
4: BF3*Et2O / acetone / Heating
5: 2) p-TsOH*H2O / 1) THF, -78 deg C 2) PhH, reflux
6: 80percent N2H4*H2O, K2CO3 / bis-(2-hydroxy-ethyl) ether / 1) 150 deg C 2) 200 deg C
With
sodium tetrahydroborate; lithium aluminium deuteride; boron trifluoride diethyl etherate; potassium carbonate; toluene-4-sulfonic acid; hydrazine hydrate; triethylamine;
In
diethyl ether; ethanol; acetone; diethylene glycol;
DOI:10.1021/jo00006a006
- Guidance literature:
-
Multi-step reaction with 5 steps
1: Et3N / diethyl ether / 25 °C
2: NaBH4 / ethanol / Heating
3: BF3*Et2O / acetone / Heating
4: 2) p-TsOH*H2O / 1) THF, -78 deg C 2) PhH, reflux
5: 80percent N2H4*H2O, K2CO3 / bis-(2-hydroxy-ethyl) ether / 1) 150 deg C 2) 200 deg C
With
sodium tetrahydroborate; boron trifluoride diethyl etherate; potassium carbonate; toluene-4-sulfonic acid; hydrazine hydrate; triethylamine;
In
diethyl ether; ethanol; acetone; diethylene glycol;
DOI:10.1021/jo00006a006
