1,3?diacetamido?5,7?dimethyladamantane

Base Information

• Chemical Name: 1,3?diacetamido?5,7?dimethyladamantane
• CAS No.: 14931-70-5
• Molecular Formula: C₁₆H₂₆N₂O₂
• Molecular Weight: 278.395
• Mol file: 14931-70-5.mol

Synonyms:

Chemical Property of 1,3?diacetamido?5,7?dimethyladamantane

Chemical Property:

Purity/Quality:

>95% ^*data from raw suppliers

5,7-Diacetamido-1,3-dimethyladamantane ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Uses: 5,7-Diacetamido-1,3-dimethyladamantane is used in the preparation of polyamides and in fibers and moldings as an antistatic agent.

Technology Process of 1,3?diacetamido?5,7?dimethyladamantane

There total 5 articles about 1,3?diacetamido?5,7?dimethyladamantane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

1,3-dimethyladamantane (702-79-4) + acetonitrile (75-05-8,26809-02-9) → 1,3?diacetamido?5,7?dimethyladamantane (14931-70-5)

Guidance literature:

1,3-dimethyladamantane; With nitric acid; at 25 ℃; for 1h;

acetonitrile; for 0.5h;

acetonitrile; With sulfuric acid; at 20 ℃; for 4h;

DOI:10.1134/S1070428017080024

Reference yield: 90.0%

1,3?dibromo?5,7?dimethyladamantane (21912-23-2) + acetonitrile (75-05-8,26809-02-9) → 1,3?diacetamido?5,7?dimethyladamantane (14931-70-5)

Guidance literature:

1,3?dibromo?5,7?dimethyladamantane; acetonitrile; With sulfuric acid; at 75 ℃;

With sodium hydroxide; at -5 ℃; pH=6 - 7; Temperature;

Reference yield:

1-acetamido-3,5-dimethyladamantane (19982-07-1) → 1,3?diacetamido?5,7?dimethyladamantane (14931-70-5)

Guidance literature:

With sodium hydroxide; sulfuric acid; In acetonitrile;

upstream raw materials:

1-acetamido-3,5-dimethyladamantane

1,3-dimethyladamantane

acetonitrile

1,3?dibromo?5,7?dimethyladamantane

Downstream raw materials:

1,3?diamino?5,7?dimethyladamantane