5,7-Dimethyl-1,3-dibromoadamantane

Base Information

• Chemical Name: 5,7-Dimethyl-1,3-dibromoadamantane
• CAS No.: 21912-23-2
• Molecular Formula: C12H18Br2
• Molecular Weight: 322.07932
• Mol file: 21912-23-2.mol

Synonyms:3,5-Dimethyl-1,7-dibromoadamantane;5,7-Dimethyl-1,3-dibromoadamantane;1,3-DIBROMO-5,7-DIMETHYLADAMANTANE

Chemical Property of 5,7-Dimethyl-1,3-dibromoadamantane

Chemical Property:

• Melting Point: 106 - 107 °C
• PSA: 0.00000
• LogP: 4.64780

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Uses: 5,7-Dimethyl-1,3-dibromoadamantane CAS:21912-23-2 is a useful building block for organic synthesis.

Technology Process of 5,7-Dimethyl-1,3-dibromoadamantane

There total 3 articles about 5,7-Dimethyl-1,3-dibromoadamantane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

1,3-dimethyladamantane (702-79-4) → 1,3?dibromo?5,7?dimethyladamantane (21912-23-2)

Guidance literature:

With bromine; iron; In 1,2-dichloro-ethane; at 25 ℃; Temperature; Reagent/catalyst; Solvent;

Reference yield:

aluminum tri-bromide + 1,3-dimethyl-5-adamantanol (707-37-9) + sodium carbonate (497-19-8) → 1,3-diethynyl-5,7-dimethyladamantane + 1,3?dibromo?5,7?dimethyladamantane (21912-23-2)

Guidance literature:

With boron tribromide; sodium sulfite; In bromine;

Reference yield:

→ 1,3?dibromo?5,7?dimethyladamantane (21912-23-2)

Guidance literature:

1,3,5,7-Tetramethylencyclooctan, Br2, CCl4;

upstream raw materials:

1,3-dimethyladamantane

1,3-dimethyl-5-adamantanol

sodium carbonate

Downstream raw materials:

5,7-dimethyladamantane-1,3-dicarboxylic acid

5,7-dimethyladamantane-1,3-diylbis(oxyethane-2,1-diyl) bis(4-nitrobenzoate)

2-(1,5-dimethyl-7-methylidenebicyclo[3.3.1]non-2-en-3-yloxy)ethyl 4-nitrobenzoate

1,3?diacetamido?5,7?dimethyladamantane