(+/-)--thioessigsaeure-S-<4-chlor-phenylester>

Base Information

Chemical Name:(+/-)--thioessigsaeure-S-<4-chlor-phenylester>
CAS No.:30032-76-9
Molecular Formula:C₂₀H₂₀Cl₂OS₂
Molecular Weight:411.416
Hs Code.:

(+/-)-<cis-2-(4-Chlor-phenylmercapto)-cyclohexyl>-thioessigsaeure-S-<4-chlor-phenylester>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)--thioessigsaeure-S-<4-chlor-phenylester>

Chemical Property:

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Technology Process of (+/-)--thioessigsaeure-S-<4-chlor-phenylester>

There total 7 articles about (+/-)--thioessigsaeure-S-<4-chlor-phenylester> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 106-54-7
p-Chlorothiophenol

: 30032-76-9
(+/-)--thioessigsaeure-S-<4-chlor-phenylester>

Guidance literature:: Multi-step reaction with 5 steps

1: piperidine / 2-methyl-propan-2-ol / Heating

2: HCl / CH₂Cl₂ / 0 °C

3: aq. HCl / Heating

4: (i) LiAlH₄, Et₂O, (ii) SOCl₂, Py, (iii) /BRN= 3587243/, DMSO, (iv) KOH, aq. EtOH

5: H₃PO₄, P₂O₅ / 150 °C

With piperidine; hydrogenchloride; phosphoric acid; phosphorus pentoxide; In dichloromethane; tert-butyl alcohol;
DOI:10.1002/hlca.19700530729

Reference yield:

: 30037-06-0,30037-07-1
(+/-)--essigsaeure

: 30032-76-9
(+/-)--thioessigsaeure-S-<4-chlor-phenylester>

Guidance literature:: With phosphoric acid; phosphorus pentoxide; at 150 ℃;
DOI:10.1002/hlca.19700530729

Reference yield:

: 1855-63-6
cyclohex-1-enecarbonitrile

: 30032-76-9
(+/-)--thioessigsaeure-S-<4-chlor-phenylester>

Guidance literature:: Multi-step reaction with 5 steps

1: piperidine / 2-methyl-propan-2-ol / Heating

2: HCl / CH₂Cl₂ / 0 °C

3: aq. HCl / Heating

4: (i) LiAlH₄, Et₂O, (ii) SOCl₂, Py, (iii) /BRN= 3587243/, DMSO, (iv) KOH, aq. EtOH

5: H₃PO₄, P₂O₅ / 150 °C

With piperidine; hydrogenchloride; phosphoric acid; phosphorus pentoxide; In dichloromethane; tert-butyl alcohol;
DOI:10.1002/hlca.19700530729