1-((1R,2S,3R,4R,5R,6R)-4-Allyloxy-2,3,5,6-tetrakis-benzyloxy-cyclohexyloxymethyl)-4-methoxy-benzene

Base Information

Chemical Name:1-((1R,2S,3R,4R,5R,6R)-4-Allyloxy-2,3,5,6-tetrakis-benzyloxy-cyclohexyloxymethyl)-4-methoxy-benzene
CAS No.:134039-20-6
Molecular Formula:C₄₅H₄₈O₇
Molecular Weight:700.872
Hs Code.:

Synonyms:

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Chemical Property of 1-((1R,2S,3R,4R,5R,6R)-4-Allyloxy-2,3,5,6-tetrakis-benzyloxy-cyclohexyloxymethyl)-4-methoxy-benzene

Chemical Property:

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Technology Process of 1-((1R,2S,3R,4R,5R,6R)-4-Allyloxy-2,3,5,6-tetrakis-benzyloxy-cyclohexyloxymethyl)-4-methoxy-benzene

There total 19 articles about 1-((1R,2S,3R,4R,5R,6R)-4-Allyloxy-2,3,5,6-tetrakis-benzyloxy-cyclohexyloxymethyl)-4-methoxy-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 34361-60-9,55123-24-5,55123-26-7,62012-78-6,104873-71-4
1,2:4,5-dicyclohexylidene-myo-inositol

: 134039-20-6
1-((1R,2S,3R,4R,5R,6R)-4-Allyloxy-2,3,5,6-tetrakis-benzyloxy-cyclohexyloxymethyl)-4-methoxy-benzene

Guidance literature:: Multi-step reaction with 11 steps

1: 68 percent / BaO/Ba(OH)2 / dimethylformamide / 72 h / 20 °C

2: 1) NaH

3: HOCH₂CH₂OH / CH₂Cl₂

4: 1) NaH

5: 0.05N HCl / methanol

6: 1) NaH

7: 1,5-cyclooctadiene-bis-IrPF₆, activated with H₂ / 1,2-dichloro-ethane

8: 0.1 HCl / CH₂Cl₂; methanol

9: 46 percent

10: 98 percent / 0.2N NaOH / dioxane; methanol; H₂O

11: 1) NaH

With hydrogenchloride; barium dihydroxide; sodium hydroxide; (1,5-cyclooctadiene)bis(methyldiphenylphosphine) iridium hexafluorophosphate; hydrogen; sodium hydride; ethylene glycol; barium(II) oxide; In 1,4-dioxane; methanol; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)92129-4

Reference yield:

: 34361-60-9,55123-24-5,55123-26-7,62012-78-6,104873-71-4
1,2:4,5-dicyclohexylidene-myo-inositol

: 134039-20-6
1-((1R,2S,3R,4R,5R,6R)-4-Allyloxy-2,3,5,6-tetrakis-benzyloxy-cyclohexyloxymethyl)-4-methoxy-benzene

Guidance literature:: Multi-step reaction with 6 steps

1: 68 percent / BaO/Ba(OH)2 / dimethylformamide / 72 h / 20 °C

2: 1) NaH

3: HOCH₂CH₂OH / CH₂Cl₂

4: 1) NaH

5: 0.05N HCl / methanol

6: 1) NaH

With hydrogenchloride; barium dihydroxide; sodium hydride; ethylene glycol; barium(II) oxide; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)92129-4

Reference yield:

: 100-39-0
benzyl bromide

: 134039-20-6
1-((1R,2S,3R,4R,5R,6R)-4-Allyloxy-2,3,5,6-tetrakis-benzyloxy-cyclohexyloxymethyl)-4-methoxy-benzene

Guidance literature:: Multi-step reaction with 8 steps

1: 1) NaH

2: 0.05N HCl / methanol

3: 1) NaH

4: 1,5-cyclooctadiene-bis-IrPF₆, activated with H₂ / 1,2-dichloro-ethane

5: 0.1 HCl / CH₂Cl₂; methanol

6: 46 percent

7: 98 percent / 0.2N NaOH / dioxane; methanol; H₂O

8: 1) NaH

With hydrogenchloride; sodium hydroxide; (1,5-cyclooctadiene)bis(methyldiphenylphosphine) iridium hexafluorophosphate; hydrogen; sodium hydride; In 1,4-dioxane; methanol; dichloromethane; water; 1,2-dichloro-ethane;
DOI:10.1016/S0040-4039(00)92129-4