2,4-Dioxohexahydropyrimidine-5-carboxylic acid

Base Information

Chemical Name:2,4-Dioxohexahydropyrimidine-5-carboxylic acid
CAS No.:92264-75-0
Molecular Formula:C5H6N2O4
Molecular Weight:158.114
Hs Code.:
Mol file:92264-75-0.mol

Synonyms:2,6-Dioxohexahydro-4-pyrimidincarbons?ure;4-pyrimidinecarboxylic acid, hexahydro-2,6-dioxo-;Acide 2,6-dioxohexahydro-4-pyrimidinecarboxylique;

Suppliers and Price of 2,4-Dioxohexahydropyrimidine-5-carboxylic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 11 raw suppliers

Chemical Property of 2,4-Dioxohexahydropyrimidine-5-carboxylic acid

Chemical Property:

Melting Point:255-256 oC
PSA：95.50000
Density:1.523 g/cm³
LogP:-0.81580

Purity/Quality:: 98%Min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,4-Dioxohexahydropyrimidine-5-carboxylic acid

There total 1 articles about 2,4-Dioxohexahydropyrimidine-5-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 23945-44-0,76821-79-9
2,4-dihydroxypyrimidine-5-carboxylic acid

: 92264-75-0
2,4-dioxohexahydropyrimidine-5-carboxylic acid

Guidance literature:: With acetic acid; platinum; Hydrogenation;

Reference yield:

: 92264-75-0
2,4-dioxohexahydropyrimidine-5-carboxylic acid

: 51940-64-8
ethyl 2,4-dichloropyrimidine-5-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine; thionyl chloride / 16 h / 15 - 75 °C

1.2: 16 h / Reflux

2.1: trichlorophosphate; N,N-diethylaniline / 105 °C

With pyridine; thionyl chloride; N,N-diethylaniline; trichlorophosphate;

Reference yield:

: 92264-75-0
2,4-dioxohexahydropyrimidine-5-carboxylic acid

: 1428759-62-9
C₃₃H₃₂ClN₇O₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: pyridine; thionyl chloride / 16 h / 15 - 75 °C

1.2: 16 h / Reflux

2.1: trichlorophosphate; N,N-diethylaniline / 105 °C

3.1: triethylamine / dichloromethane; tetrahydrofuran / 3 h / -78 °C

4.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 - 5 °C

5.1: manganese(IV) oxide / tetrahydrofuran / 1 h / 40 °C

6.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dimethyl sulfoxide

7.1: trifluoroacetic acid / dimethyl sulfoxide / 0.08 h

7.2: 16 h / 110 °C

With pyridine; manganese(IV) oxide; lithium aluminium tetrahydride; thionyl chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; trifluoroacetic acid; N,N-diethylaniline; trichlorophosphate; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide;