1-phenyldimethylsilyl-1-trimethylsilyl-3-phenylpropadiene

Base Information

Chemical Name:1-phenyldimethylsilyl-1-trimethylsilyl-3-phenylpropadiene
CAS No.:79194-26-6
Molecular Formula:C₂₀H₂₆Si₂
Molecular Weight:322.597
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-phenyldimethylsilyl-1-trimethylsilyl-3-phenylpropadiene

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Technology Process of 1-phenyldimethylsilyl-1-trimethylsilyl-3-phenylpropadiene

There total 5 articles about 1-phenyldimethylsilyl-1-trimethylsilyl-3-phenylpropadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 79194-25-5
1-dimethylphenylsilyl-3-trimethylsilyl-3-phenylpropyne

: 79194-26-6
1-phenyldimethylsilyl-1-trimethylsilyl-3-phenylpropadiene

Guidance literature:: In cyclohexane; for 8h; Irradiation;

Reference yield:

: 673-32-5
1-Phenylprop-1-yne

: 79194-26-6
1-phenyldimethylsilyl-1-trimethylsilyl-3-phenylpropadiene

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) TMEDA, butyllithium / 1.) hexane, -70 deg C to room temperature, reflux 15 min; 2.) reflux 30 min

2: 1.) TMEDA, butyllithium / 1.) hexane, -70 deg C to room temperature, reflux 15 min; 2.) reflux 30 min

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine;

Reference yield:

: 768-33-2
phenyldimethylsilyl chloride

: 79194-26-6
1-phenyldimethylsilyl-1-trimethylsilyl-3-phenylpropadiene

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) TMEDA, butyllithium / 1.) hexane, -70 deg C to room temperature, reflux 15 min; 2.) reflux 30 min

2: 1.) TMEDA, butyllithium / 1.) hexane, -70 deg C to room temperature, reflux 15 min; 2.) reflux 30 min

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine;