C₂₃H₂₉N₅O₃

Base Information

• Chemical Name: C₂₃H₂₉N₅O₃
• CAS No.: 1404065-62-8
• Molecular Formula: C₂₃H₂₉N₅O₃
• Molecular Weight: 423.515
• Mol file: 1404065-62-8.mol

Synonyms:

Chemical Property of C₂₃H₂₉N₅O₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₃H₂₉N₅O₃

There total 5 articles about C₂₃H₂₉N₅O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C28H37N5O5 (1404065-47-9) → C23H29N5O3 (1404065-62-8)

Guidance literature:

With hydrogenchloride; In ethyl acetate; at 20 ℃; for 4h;

DOI:10.1016/j.bmcl.2012.07.077

Reference yield:

4-amino-6-methyl-5-nitropyridazin-3(2H)-one (202277-51-8) → C23H29N5O3 (1404065-62-8)

Guidance literature:

Multi-step reaction with 4 steps

1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 100 - 110 °C

2: acetic acid; iron / 12 h / Reflux

3: sulfur / 5,5-dimethyl-1,3-cyclohexadiene / 2 h / 160 °C

4: hydrogenchloride / ethyl acetate / 4 h / 20 °C

With hydrogenchloride; iron; potassium carbonate; sulfur; acetic acid; In 5,5-dimethyl-1,3-cyclohexadiene; ethyl acetate; N,N-dimethyl-formamide;

DOI:10.1016/j.bmcl.2012.07.077

Reference yield:

4-amino-2-cyclohexyl-6-methyl-5-nitropyridazin-3(2H)-one (1404065-14-0) → C23H29N5O3 (1404065-62-8)

Guidance literature:

Multi-step reaction with 3 steps

1: acetic acid; iron / 12 h / Reflux

2: sulfur / 5,5-dimethyl-1,3-cyclohexadiene / 2 h / 160 °C

3: hydrogenchloride / ethyl acetate / 4 h / 20 °C

With hydrogenchloride; iron; sulfur; acetic acid; In 5,5-dimethyl-1,3-cyclohexadiene; ethyl acetate;

DOI:10.1016/j.bmcl.2012.07.077

upstream raw materials:

3-methyl-4,5-dihydro-6-oxopyridazine

4-amino-6-methylpyridazin-3(2H)-one

4-amino-6-methyl-5-nitropyridazin-3(2H)-one

4-amino-2-cyclohexyl-6-methyl-5-nitropyridazin-3(2H)-one

Refernces