[8-(diethoxy-phosphorylmethyl)-15-phenyl-15-thioxo-1,5,8,12-tetraaza-15λ⁵-phospha-bicyclo[10.2.1]pentadec-5-ylmethyl]-phosphonic acid diethyl ester

Base Information

• Chemical Name: [8-(diethoxy-phosphorylmethyl)-15-phenyl-15-thioxo-1,5,8,12-tetraaza-15λ⁵-phospha-bicyclo[10.2.1]pentadec-5-ylmethyl]-phosphonic acid diethyl ester
• CAS No.: 917838-69-8
• Molecular Formula: C₂₆H₄₉N₄O₆P₃S
• Molecular Weight: 638.686

Synonyms:

Chemical Property of [8-(diethoxy-phosphorylmethyl)-15-phenyl-15-thioxo-1,5,8,12-tetraaza-15λ⁵-phospha-bicyclo[10.2.1]pentadec-5-ylmethyl]-phosphonic acid diethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Useful:

Technology Process of [8-(diethoxy-phosphorylmethyl)-15-phenyl-15-thioxo-1,5,8,12-tetraaza-15λ⁵-phospha-bicyclo[10.2.1]pentadec-5-ylmethyl]-phosphonic acid diethyl ester

There total 2 articles about [8-(diethoxy-phosphorylmethyl)-15-phenyl-15-thioxo-1,5,8,12-tetraaza-15λ⁵-phospha-bicyclo[10.2.1]pentadec-5-ylmethyl]-phosphonic acid diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

15-phenyl-1,5,8,12-tetraaza-15λ5-phosphabicyclo[10.2.1]pentadecane-15-thione (917838-66-5,917905-60-3) + formaldehyd (50-00-0,30525-89-4,61233-19-0) + triethyl phosphite (122-52-1) → [8-(diethoxy-phosphorylmethyl)-15-phenyl-15-thioxo-1,5,8,12-tetraaza-15λ5-phospha-bicyclo[10.2.1]pentadec-5-ylmethyl]-phosphonic acid diethyl ester (917838-69-8)

Guidance literature:

at 40 ℃;

DOI:10.1135/cccc20060337

Reference yield:

1,4,8,11-Tetraazacyclotetradecane (295-37-4) → [8-(diethoxy-phosphorylmethyl)-15-phenyl-15-thioxo-1,5,8,12-tetraaza-15λ5-phospha-bicyclo[10.2.1]pentadec-5-ylmethyl]-phosphonic acid diethyl ester (917838-69-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 42 percent / Et₃N / CHCl₃ / 72 h / 20 °C

2: 81 percent / 40 °C

With triethylamine; In chloroform; 2: Mannich reaction;

DOI:10.1135/cccc20060337

upstream raw materials:

15-phenyl-1,5,8,12-tetraaza-15λ⁵-phosphabicyclo[10.2.1]pentadecane-15-thione

formaldehyd

triethyl phosphite

1,4,8,11-Tetraazacyclotetradecane

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