Technology Process of C30H25N3O2
There total 4 articles about C30H25N3O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: ammonium hydroxide / water; ethanol / 2 h / 0 - 20 °C / Inert atmosphere
2: neat (no solvent) / 7 h / 120 - 140 °C / Inert atmosphere
3: water / 4 - 5 h / 20 °C / Inert atmosphere; UV-irradiation
With
ammonium hydroxide;
In
ethanol; water;
DOI:10.1021/ic400676j
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: boron tribromide / dichloromethane / 12 h / 0 °C / Inert atmosphere
1.2: 1 h / 20 °C / Inert atmosphere
2.1: neat (no solvent) / 7 h / 120 - 140 °C / Inert atmosphere
3.1: water / 4 - 5 h / 20 °C / Inert atmosphere; UV-irradiation
With
boron tribromide;
In
dichloromethane; water;
DOI:10.1021/ic400676j
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / water; tetrahydrofuran / 36 h / 85 - 90 °C / Inert atmosphere; Saturated solution
2.1: boron tribromide / dichloromethane / 12 h / 0 °C / Inert atmosphere
2.2: 1 h / 20 °C / Inert atmosphere
3.1: neat (no solvent) / 7 h / 120 - 140 °C / Inert atmosphere
4.1: water / 4 - 5 h / 20 °C / Inert atmosphere; UV-irradiation
With
tetrakis(triphenylphosphine) palladium(0); boron tribromide; potassium carbonate;
In
tetrahydrofuran; dichloromethane; water;
1.1: |Suzuki Coupling;
DOI:10.1021/ic400676j