but-3-yn-2-yl benzoate

Base Information

• Chemical Name: but-3-yn-2-yl benzoate
• CAS No.: 29333-27-5
• Molecular Formula: C₁₁H₁₀O₂
• Molecular Weight: 174.199
• Mol file: 29333-27-5.mol

Synonyms:

Chemical Property of but-3-yn-2-yl benzoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of but-3-yn-2-yl benzoate

There total 4 articles about but-3-yn-2-yl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

benzoyl chloride (98-88-4) + but-3-yn-2-ol (2028-63-9) → but-3-yn-2-yl benzoate (29333-27-5,7342-11-2)

Guidance literature:

In pyridine; at 20 ℃; for 2h;

DOI:10.1016/S0957-4166(02)00121-0

Reference yield: 75.0%

but-3-yn-2-ol (2028-63-9) + benzoic acid (65-85-0,8013-63-6) → but-3-yn-2-yl benzoate (29333-27-5,7342-11-2)

Guidance literature:

With graphene oxide; In 1,2-dichloro-ethane; at 100 ℃; for 24h;

DOI:10.1055/s-0036-1588399

Reference yield:

benzoyl chloride (98-88-4) → but-3-yn-2-yl benzoate (29333-27-5,7342-11-2)

Guidance literature:

With sodium hydroxide; water; at -10 ℃;

upstream raw materials:

benzoyl chloride

but-3-yn-2-ol

benzoic acid

Downstream raw materials:

Benzoic acid 1-methyl-2-piperidin-1-yl-allyl ester

Benzoic acid 1-methyl-2-morpholin-4-yl-allyl ester

2-methyl-1-phenyl-2,3-butadien-1-ol

(R)-(+)-3-butyn-2-ol