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((E)-Hept-1-enyl)-phenyl-diazene

Base Information
  • Chemical Name:((E)-Hept-1-enyl)-phenyl-diazene
  • CAS No.:127680-05-1
  • Molecular Formula:C13H18N2
  • Molecular Weight:202.299
  • Hs Code.:
((E)-Hept-1-enyl)-phenyl-diazene

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Chemical Property of ((E)-Hept-1-enyl)-phenyl-diazene
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Technology Process of ((E)-Hept-1-enyl)-phenyl-diazene

There total 4 articles about ((E)-Hept-1-enyl)-phenyl-diazene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With potassium; tert-butyl alcohol; In diethyl ether; at -55 ℃; for 0.5h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1016/S0040-4020(01)85424-7
Guidance literature:
Multi-step reaction with 2 steps
2: 1) potassium, t-butyl alcohol / diethyl ether / 0.5 h / -55 °C
With potassium; tert-butyl alcohol; In diethyl ether;
DOI:10.1016/S0040-4020(01)85424-7
Guidance literature:
With iodine; sodium hydrogencarbonate; Yield given. Multistep reaction. Further byproducts given. Title compound not separated from byproducts; 1) 50 deg C, 2 h, 2) water, 50-60 deg C, 10 min;
DOI:10.1016/S0040-4020(01)85424-7
upstream raw materials:

pyridine

heptanal phenylhydrazone

C20H26N2O2S

Downstream raw materials:

((Z)-Hept-1-enyl)-phenyl-diazene

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