2,6-dimorpholino-4-phenyl-1,3,5-oxadiazinium acetonitrile trichlorocobaltate(II)

Base Information

Chemical Name:2,6-dimorpholino-4-phenyl-1,3,5-oxadiazinium acetonitrile trichlorocobaltate(II)
CAS No.:139940-06-0
Molecular Formula:C₂H₃Cl₃CoN*C₁₇H₂₁N₄O₃
Molecular Weight:535.783
Hs Code.:

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Chemical Property of 2,6-dimorpholino-4-phenyl-1,3,5-oxadiazinium acetonitrile trichlorocobaltate(II)

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Technology Process of 2,6-dimorpholino-4-phenyl-1,3,5-oxadiazinium acetonitrile trichlorocobaltate(II)

There total 2 articles about 2,6-dimorpholino-4-phenyl-1,3,5-oxadiazinium acetonitrile trichlorocobaltate(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 40398-30-9
N-(morpholinothiocarbonyl)benzamide

: cobalt(II) chloride hexahydrate

: 75-05-8,26809-02-9
acetonitrile

: 139940-06-0
2,6-dimorpholino-4-phenyl-1,3,5-oxadiazinium acetonitrile trichlorocobaltate(II)

Guidance literature:: With SOCl₂; In acetonitrile; byproducts: S; slow addn. of organic ligand to SOCl2 soln.; refluxing, 15 min; cooling; separation of S; addn. of CoCl2 soln.; boiling for a short period of time; cooling, evapn. to a small volume; standing at 0°C, 2 d; pptn.; filtration, recrystn. (CH3CN); drying in air; elem. anal.;

Reference yield: 45.0%

: tris(N-morpholine-N’-benzoylthioureato)cobalt(III)

: 75-05-8,26809-02-9
acetonitrile

: 139940-06-0
2,6-dimorpholino-4-phenyl-1,3,5-oxadiazinium acetonitrile trichlorocobaltate(II)

Guidance literature:: With SOCl₂; In acetonitrile; addn. of SOCl2 with stirring to Co complex suspension; boiling for a short period of time; cooling, evapn. to a small volume; standing at 0°C, 2 d; pptn.; filtration, recrystn. (CH3CN); drying in air; elem. anal.;