benzodioxine-(1,3)> carboxylate-2 de methyle cis

Base Information

Chemical Name: benzodioxine-(1,3)> carboxylate-2 de methyle cis
CAS No.:67059-82-9
Molecular Formula:C₁₇H₁₄Cl₂O₄
Molecular Weight:353.202
Hs Code.:

<chloro-6 (chloro-3 phenyl)-4 methyl-4 <4H> benzodioxine-(1,3)> carboxylate-2 de methyle cis

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Chemical Property of benzodioxine-(1,3)> carboxylate-2 de methyle cis

Chemical Property:

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Technology Process of benzodioxine-(1,3)> carboxylate-2 de methyle cis

There total 6 articles about benzodioxine-(1,3)> carboxylate-2 de methyle cis which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1450-74-4
5-chloro-2-hydroxyacetophenone

: 67059-82-9,67059-83-0,71980-75-1,86609-07-6,86616-98-0
(2RS, 4RS) benzodioxine-(1,3)> carboxylate-2 de methyle

Guidance literature:: Multi-step reaction with 3 steps

1: 66 percent / 50percent NaH/mineral oil / tetrahydrofuran / Ambient temperature

2: 50percent NaH/mineral oil, 18 crown 6 / dioxane / 3 h / 65 °C

3: 97 percent / Redex CF resin

With 18-crown-6 ether; Redex CF resin; sodium hydride; mineral oil; In tetrahydrofuran; 1,4-dioxane;

Reference yield:

: 1450-74-4
5-chloro-2-hydroxyacetophenone

: 67059-82-9,67059-83-0,71980-75-1,86609-07-6,86616-98-0
benzodioxine-(1,3)> carboxylate-2 de methyle cis

Guidance literature:: Multi-step reaction with 3 steps

1: 66 percent / 50percent NaH/mineral oil / tetrahydrofuran / Ambient temperature

2: 50percent NaH/mineral oil, 18 crown 6 / dioxane / 3 h / 65 °C

3: Redex CF resin

With 18-crown-6 ether; Redex CF resin; sodium hydride; mineral oil; In tetrahydrofuran; 1,4-dioxane;

Reference yield:

: 67059-80-7
chloro-5 α-(chloro-3-phenyl) hydroxy-2 α-methyl benzene methanol

: 67059-82-9,67059-83-0,71980-75-1,86609-07-6,86616-98-0
(2RS, 4RS) benzodioxine-(1,3)> carboxylate-2 de methyle

Guidance literature:: Multi-step reaction with 2 steps

1: 50percent NaH/mineral oil, 18 crown 6 / dioxane / 3 h / 65 °C

2: 97 percent / Redex CF resin

With 18-crown-6 ether; Redex CF resin; sodium hydride; mineral oil; In 1,4-dioxane;