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Technology Process of C5(C6H5)2(C10H7)2ORu(CO)2CH3CHCH3OH

C5(C6H5)2(C10H7)2ORu(CO)2CH3CHCH3OH

Base Information
  • Chemical Name:C5(C6H5)2(C10H7)2ORu(CO)2CH3CHCH3OH
  • CAS No.:359445-55-9
  • Molecular Formula:C42H32O4Ru
  • Molecular Weight:701.784
  • Hs Code.:
C<sub>5</sub>(C<sub>6</sub>H<sub>5</sub>)2(C<sub>10</sub>H<sub>7</sub>)2ORu(CO)2CH<sub>3</sub>CHCH<sub>3</sub>OH

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Chemical Property of C5(C6H5)2(C10H7)2ORu(CO)2CH3CHCH3OH
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Technology Process of C5(C6H5)2(C10H7)2ORu(CO)2CH3CHCH3OH

There total 1 articles about C5(C6H5)2(C10H7)2ORu(CO)2CH3CHCH3OH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

C<sub>5</sub>(C<sub>6</sub>H<sub>5</sub>)3(C<sub>10</sub>H<sub>7</sub>)ORu(CO)3

C5(C6H5)3(C10H7)ORu(CO)3

acetone
67-64-1

acetone

C<sub>5</sub>(C<sub>6</sub>H<sub>5</sub>)2(C<sub>10</sub>H<sub>7</sub>)2ORu(CO)2CH<sub>3</sub>CHCH<sub>3</sub>OH
359445-55-9

C5(C6H5)2(C10H7)2ORu(CO)2CH3CHCH3OH

([2,5-bis(1-naphthyl)-3,4-diphenyl(η5-C4CO)]2)Ru2(CO)4(μ-H)

([2,5-bis(1-naphthyl)-3,4-diphenyl(η5-C4CO)]2)Ru2(CO)4(μ-H)

Guidance literature:
With Na2CO3; In water; acetone; an acetone soln. of complex was treated with aq. Na2CO3 at 20°C for 1 h, stirred for 1 h, cooled to 0°C; concd., the residue was extd. with CH2Cl2, evapd., chromd. on silica gelwith CH2Cl2/ethyl acetate, recrystd. from CH2Cl2-hexane; elem. anal.;
DOI:10.1021/om0103198
upstream raw materials:

acetone

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