Diethyl butyl(prop-2-en-1-yl)propanedioate

Base Information

Chemical Name:Diethyl butyl(prop-2-en-1-yl)propanedioate
CAS No.:1575-76-4
Molecular Formula:C14H24 O4
Molecular Weight:256.342
Hs Code.:
NSC Number:128928
DSSTox Substance ID:DTXSID20935683
Nikkaji Number:J2.281.837F
Wikidata:Q82911755
Mol file:1575-76-4.mol

Synonyms:1575-76-4;diethyl butyl(prop-2-en-1-yl)propanedioate;NSC128928;SCHEMBL9478485;DTXSID20935683;NSC-128928

Suppliers and Price of Diethyl butyl(prop-2-en-1-yl)propanedioate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Diethyl butyl(prop-2-en-1-yl)propanedioate

Chemical Property:

Vapor Pressure:0.00363mmHg at 25°C
Boiling Point:281.1°C at 760 mmHg
Flash Point:123.4°C
Density:0.979g/cm³
XLogP3:3.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:11
Exact Mass:256.16745924
Heavy Atom Count:18
Complexity:266

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCC(CC=C)(C(=O)OCC)C(=O)OCC

Technology Process of Diethyl butyl(prop-2-en-1-yl)propanedioate

There total 4 articles about Diethyl butyl(prop-2-en-1-yl)propanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 109-65-9
1-bromo-butane

: 2049-80-1
(2-propenyl)propanedioic acid diethyl ester

: 1575-76-4
2-butyl-2-ethoxycarbonylpenten-4-oic acid ethyl ester

Guidance literature:: With sodium ethanolate; In ethanol; for 1h; Heating;
DOI:10.1021/ja047320t

Reference yield:

: 3195-24-2
diallylmalonic acid diethyl ester

: 1575-76-4
2-butyl-2-ethoxycarbonylpenten-4-oic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent Spectr_. / Et₃Al; RuCl₂(PPh₃)3 / toluene / 36 h / 20 °C

2: 69 percent / NaOEt / ethanol / 1 h / Heating

With tris(triphenylphosphine)ruthenium(II) chloride; triethylaluminum; sodium ethanolate; In ethanol; toluene;
DOI:10.1021/ja047320t