8-Bromo-7-methoxyquinoline

Base Information

• Chemical Name: 8-Bromo-7-methoxyquinoline
• CAS No.: 36023-06-0
• Molecular Formula: C₁₀H₈BrNO
• Molecular Weight: 238.084
• Hs Code.: 2933499090
• Mol file: 36023-06-0.mol

Synonyms:7-Methoxy-8-bromoquinoline

Chemical Property of 8-Bromo-7-methoxyquinoline

Chemical Property:

• PSA: 22.12000
• Density: 1.516
• LogP: 3.00590
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

99% ^*data from raw suppliers

8-Bromo-7-methoxyquinoline ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 8-Bromo-7-methoxyquinoline

There total 4 articles about 8-Bromo-7-methoxyquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.1%

7-methoxyquinoline (4964-76-5) → 8-bromo-7-methoxyquinoline (36023-06-0)

Guidance literature:

With N-Bromosuccinimide; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1039/C7CC01635B

Reference yield:

8-bromo-7-hydroxyquinoline (90224-71-8) + methyl iodide (74-88-4) → 8-bromo-7-methoxyquinoline (36023-06-0)

Guidance literature:

With potassium carbonate; In acetone; for 4h; Reflux;

Reference yield:

m-Anisidine (536-90-3,918666-97-4) → 8-bromo-7-methoxyquinoline (36023-06-0)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium 3-nitrobenzenesulfonate; ferrous(II) sulfate heptahydrate / methanesulfonic acid / 16 h / 118 - 135 °C

2: N-Bromosuccinimide / dichloromethane / 0 - 20 °C / Inert atmosphere

With ferrous(II) sulfate heptahydrate; N-Bromosuccinimide; sodium 3-nitrobenzenesulfonate; In methanesulfonic acid; dichloromethane;

DOI:10.1039/C7CC01635B

upstream raw materials:

8-bromo-7-hydroxyquinoline

methyl iodide

7-methoxyquinoline

m-Anisidine

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