Benzyl-O-(2-acetamido-3,4,6-tri-O-benzyl-2-desoxy-β-D-mannopyranosyl)-(1->3)-O-(2-acetamido-4-O-acetyl-2,6-didesoxy-α-L-galactopyranosyl)-(1->3)-2-acetamido-4,6-O-benzyliden-2-desoxy-β-D-galactopyranosid

Base Information

Chemical Name:Benzyl-O-(2-acetamido-3,4,6-tri-O-benzyl-2-desoxy-β-D-mannopyranosyl)-(1->3)-O-(2-acetamido-4-O-acetyl-2,6-didesoxy-α-L-galactopyranosyl)-(1->3)-2-acetamido-4,6-O-benzyliden-2-desoxy-β-D-galactopyranosid
CAS No.:103751-42-4
Molecular Formula:C₆₁H₇₁N₃O₁₆
Molecular Weight:1102.25
Hs Code.:

Benzyl-O-(2-acetamido-3,4,6-tri-O-benzyl-2-desoxy-β-D-mannopyranosyl)-(1->3)-O-(2-acetamido-4-O-acetyl-2,6-didesoxy-α-L-galactopyranosyl)-(1->3)-2-acetamido-4,6-O-benzyliden-2-desoxy-β-D-galactopyranosid

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Chemical Property of Benzyl-O-(2-acetamido-3,4,6-tri-O-benzyl-2-desoxy-β-D-mannopyranosyl)-(1->3)-O-(2-acetamido-4-O-acetyl-2,6-didesoxy-α-L-galactopyranosyl)-(1->3)-2-acetamido-4,6-O-benzyliden-2-desoxy-β-D-galactopyranosid

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Technology Process of Benzyl-O-(2-acetamido-3,4,6-tri-O-benzyl-2-desoxy-β-D-mannopyranosyl)-(1->3)-O-(2-acetamido-4-O-acetyl-2,6-didesoxy-α-L-galactopyranosyl)-(1->3)-2-acetamido-4,6-O-benzyliden-2-desoxy-β-D-galactopyranosid

There total 6 articles about Benzyl-O-(2-acetamido-3,4,6-tri-O-benzyl-2-desoxy-β-D-mannopyranosyl)-(1->3)-O-(2-acetamido-4-O-acetyl-2,6-didesoxy-α-L-galactopyranosyl)-(1->3)-2-acetamido-4,6-O-benzyliden-2-desoxy-β-D-galactopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 103751-42-4
Benzyl-O-(2-acetamido-3,4,6-tri-O-benzyl-2-desoxy-β-D-mannopyranosyl)-(1->3)-O-(2-acetamido-4-O-acetyl-2,6-didesoxy-α-L-galactopyranosyl)-(1->3)-2-acetamido-4,6-O-benzyliden-2-desoxy-β-D-galactopyranosid

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / p-TsOH / acetonitrile / 1 h / Ambient temperature

3: 1) H₂S-gas / 1.) pyridine, H₂O, 18h, r.t. 2.) pyridine, 0 deg C, 6h

With hydrogen sulfide; toluene-4-sulfonic acid; In acetonitrile;

Reference yield:

: 1,4-Di-O-acetyl-2-azido-3-O-(2-azido-3,4,6-tri-O-benzyl-2-desoxy-β-D-mannopyranosyl)-2,6-didesoxy-α,β-L-galactopyranose

: 103751-42-4
Benzyl-O-(2-acetamido-3,4,6-tri-O-benzyl-2-desoxy-β-D-mannopyranosyl)-(1->3)-O-(2-acetamido-4-O-acetyl-2,6-didesoxy-α-L-galactopyranosyl)-(1->3)-2-acetamido-4,6-O-benzyliden-2-desoxy-β-D-galactopyranosid

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / TiBr₄ / CH₂Cl₂; ethyl acetate / 1 h / Ambient temperature

3: 1) H₂S-gas / 1.) pyridine, H₂O, 18h, r.t. 2.) pyridine, 0 deg C, 6h

With hydrogen sulfide; titanium(IV) bromide; In dichloromethane; ethyl acetate;

Reference yield:

: 97604-42-7,166907-09-1
benzyl 2-azido-2-deoxy-β-D-galactopyranoside

: 103751-42-4
Benzyl-O-(2-acetamido-3,4,6-tri-O-benzyl-2-desoxy-β-D-mannopyranosyl)-(1->3)-O-(2-acetamido-4-O-acetyl-2,6-didesoxy-α-L-galactopyranosyl)-(1->3)-2-acetamido-4,6-O-benzyliden-2-desoxy-β-D-galactopyranosid

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / p-TsOH / acetonitrile / 1 h / Ambient temperature

3: 1) H₂S-gas / 1.) pyridine, H₂O, 18h, r.t. 2.) pyridine, 0 deg C, 6h

With hydrogen sulfide; toluene-4-sulfonic acid; In acetonitrile;