(+/-)-1-<(1α,3β,4α)-3-hydroxy-4-(hydroxymethyl)cyclopentyl>-2,4-(1H,3H)pyrimidinedione dibenzoate

Base Information

• Chemical Name: (+/-)-1-<(1α,3β,4α)-3-hydroxy-4-(hydroxymethyl)cyclopentyl>-2,4-(1H,3H)pyrimidinedione dibenzoate
• CAS No.: 69975-18-4
• Molecular Formula: C₂₄H₂₂N₂O₆
• Molecular Weight: 434.448
• Mol file: 69975-18-4.mol

Synonyms:

Chemical Property of (+/-)-1-<(1α,3β,4α)-3-hydroxy-4-(hydroxymethyl)cyclopentyl>-2,4-(1H,3H)pyrimidinedione dibenzoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (+/-)-1-<(1α,3β,4α)-3-hydroxy-4-(hydroxymethyl)cyclopentyl>-2,4-(1H,3H)pyrimidinedione dibenzoate

There total 1 articles about (+/-)-1-<(1α,3β,4α)-3-hydroxy-4-(hydroxymethyl)cyclopentyl>-2,4-(1H,3H)pyrimidinedione dibenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(+/-)-1-<(1β,3α,4β)-3-hydroxy-4-(hydroxymethyl)cyclopentyl>-2,4(1H,3H)-pyrimidinedione (62102-28-7) + benzoyl chloride (98-88-4) → (+/-)-1-<(1α,3β,4α)-3-hydroxy-4-(hydroxymethyl)cyclopentyl>-2,4-(1H,3H)pyrimidinedione dibenzoate (69975-18-4)

Guidance literature:

With hydrogenchloride; Yield given. Multistep reaction; 1.) pyridine, 2.) ethanol, water, reflux, 15 h.;

DOI:10.1002/jhet.5570170228

Reference yield:

(+/-)-1-<(1α,3β,4α)-3-hydroxy-4-(hydroxymethyl)cyclopentyl>-2,4-(1H,3H)pyrimidinedione dibenzoate (69975-18-4) → C24H21ClN2O5 (69975-19-5)

Guidance literature:

With thionyl chloride; N,N-dimethyl-formamide; In chloroform; Heating;

DOI:10.1002/jhet.5570170228

upstream raw materials:

(+/-)-1-<(1β,3α,4β)-3-hydroxy-4-(hydroxymethyl)cyclopentyl>-2,4(1H,3H)-pyrimidinedione

benzoyl chloride

Downstream raw materials:

C₂₄H₂₁ClN₂O₅