Technology Process of C29H34N2O5
There total 5 articles about C29H34N2O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 83 percent / potassium carbonate / 1.) 20 deg C, 8 h, 2.) 45 deg C, 8 h
2: p-toluenesulfonic acid / benzene / 5 h / Heating
3: 2.01 g / lithium aluminum hydride (LAH) / tetrahydrofuran / 4 h / 20 °C
4: PCC, sodium acetate / CH2Cl2 / 1.25 h / 20 °C
5: methanol / 4 h / Ambient temperature
With
lithium aluminium tetrahydride; sodium acetate; potassium carbonate; toluene-4-sulfonic acid; pyridinium chlorochromate;
In
tetrahydrofuran; methanol; dichloromethane; benzene;
DOI:10.1021/jo00280a021
- Guidance literature:
-
Multi-step reaction with 2 steps
1: PCC, sodium acetate / CH2Cl2 / 1.25 h / 20 °C
2: methanol / 4 h / Ambient temperature
With
sodium acetate; pyridinium chlorochromate;
In
methanol; dichloromethane;
DOI:10.1021/jo00280a021
- Guidance literature:
-
Multi-step reaction with 4 steps
1: p-toluenesulfonic acid / benzene / 5 h / Heating
2: 2.01 g / lithium aluminum hydride (LAH) / tetrahydrofuran / 4 h / 20 °C
3: PCC, sodium acetate / CH2Cl2 / 1.25 h / 20 °C
4: methanol / 4 h / Ambient temperature
With
lithium aluminium tetrahydride; sodium acetate; toluene-4-sulfonic acid; pyridinium chlorochromate;
In
tetrahydrofuran; methanol; dichloromethane; benzene;
DOI:10.1021/jo00280a021
