(1S,4S)-2,5-Diazabicyclo<2.2.1>heptane dihydrobromide

Base Information

Chemical Name:(1S,4S)-2,5-Diazabicyclo<2.2.1>heptane dihydrobromide
CAS No.:116258-16-3
Molecular Formula:2BrH*C₅H₁₀N₂
Molecular Weight:259.972
Hs Code.:

Synonyms:

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Chemical Property of (1S,4S)-2,5-Diazabicyclo<2.2.1>heptane dihydrobromide

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Technology Process of (1S,4S)-2,5-Diazabicyclo<2.2.1>heptane dihydrobromide

There total 2 articles about (1S,4S)-2,5-Diazabicyclo<2.2.1>heptane dihydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 100944-15-8,134003-82-0,116258-17-4
(1S,4S)-2-Benzyl-2,5-diazabicyclo<2.2.1>heptane dihydrobromide

: 100944-14-7,116258-16-3,132747-20-7
(1S,4S)-2,5-Diazabicyclo<2.2.1>heptane dihydrobromide

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; water; for 1h; under 3361.55 Torr;
DOI:10.1002/ejoc.200700785

Reference yield:

: 5234-72-0,59436-75-8
(1S,4S)-5-Benzyl-2-tosyl-2,5-diazabicyclo<2.2.1>heptane

: 100944-14-7,116258-16-3,132747-20-7
(1S,4S)-2,5-Diazabicyclo<2.2.1>heptane dihydrobromide

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / red phosphorus, 48 percent aq. hydrobromic acid / H₂O / 24 h / Heating

2: 90 percent / hydrogen / 10 percent Pd-C / methanol; H₂O / 24 h / 3620.04 Torr

With phosphorus; hydrogen bromide; hydrogen; palladium on activated charcoal; In methanol; water;
DOI:10.1055/s-1990-27056

Reference yield: 86.0%

: 553-86-6
benzofuran-2(3H)-one

: 100944-14-7,116258-16-3,132747-20-7
(1S,4S)-2,5-Diazabicyclo<2.2.1>heptane dihydrobromide

: 1032278-89-9
(1S,4S)-2,5-bis[2-(2-hydroxyphenyl)acetyl]diazabicyclo[2.2.1]heptane

Guidance literature:: (1S,4S)-2,5-Diazabicyclo<2.2.1>heptane dihydrobromide; With potassium hydroxide; In methanol; at 5 - 10 ℃; for 1h;

benzofuran-2(3H)-one; In toluene; at 20 ℃; for 0.0833333h; Further stages.;
DOI:10.1002/ejoc.200700785