C₁₃H₁₄BrN₃O

Base Information

Chemical Name:C₁₃H₁₄BrN₃O
CAS No.:1049639-30-6
Molecular Formula:C₁₃H₁₄BrN₃O
Molecular Weight:308.178
Hs Code.:

C<sub>13</sub>H<sub>14</sub>BrN<sub>3</sub>O

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₃H₁₄BrN₃O

Chemical Property:

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Technology Process of C₁₃H₁₄BrN₃O

There total 7 articles about C₁₃H₁₄BrN₃O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1370656-89-5
C₁₂H₁₄BrNO₂

: 1049639-30-6
C₁₃H₁₄BrN₃O

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydrogencarbonate / dichloromethane; water

2: N-ethyl-N,N-diisopropylamine / 70 °C

3: tert.-butylhydroperoxide; ammonium hydroxide

With tert.-butylhydroperoxide; ammonium hydroxide; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; In dichloromethane; water;
DOI:10.1016/j.bmcl.2012.02.013

Reference yield:

: 1049669-09-1
C₁₁H₁₂BrNO₂

: 1049639-30-6
C₁₃H₁₄BrN₃O

Guidance literature:: Multi-step reaction with 4 steps

2: sodium hydrogencarbonate / dichloromethane; water

3: N-ethyl-N,N-diisopropylamine / 70 °C

4: tert.-butylhydroperoxide; ammonium hydroxide

With tert.-butylhydroperoxide; ammonium hydroxide; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; In dichloromethane; water;
DOI:10.1016/j.bmcl.2012.02.013

Reference yield:

: 1711-09-7
3-bromobenzoyl chloride

: 1049639-30-6
C₁₃H₁₄BrN₃O

Guidance literature:: Multi-step reaction with 7 steps

1: copper(l) chloride; lithium chloride / -60 °C

2: potassium cyanide / 120 °C

3: water; potassium hydroxide / 24 h / 185 °C

5: sodium hydrogencarbonate / dichloromethane; water

6: N-ethyl-N,N-diisopropylamine / 70 °C

7: tert.-butylhydroperoxide; ammonium hydroxide

With tert.-butylhydroperoxide; potassium cyanide; ammonium hydroxide; water; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; copper(l) chloride; lithium chloride; potassium hydroxide; In dichloromethane; water; 2: Bucherer-Bergs reaction;
DOI:10.1016/j.bmcl.2012.02.013