Acetamide, N-[(1S)-1-methyl-2-(3-methylphenyl)ethyl]-

Base Information

Chemical Name:Acetamide, N-[(1S)-1-methyl-2-(3-methylphenyl)ethyl]-
CAS No.:1132758-31-6
Molecular Formula:C12H17NO
Molecular Weight:191.273
Hs Code.:

Synonyms:

Suppliers and Price of Acetamide, N-[(1S)-1-methyl-2-(3-methylphenyl)ethyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Acetamide, N-[(1S)-1-methyl-2-(3-methylphenyl)ethyl]-

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Acetamide, N-[(1S)-1-methyl-2-(3-methylphenyl)ethyl]-

There total 4 articles about Acetamide, N-[(1S)-1-methyl-2-(3-methylphenyl)ethyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 69390-43-8
(Z)-N-(1-m-tolylprop-1-en-2-yl)acetamide

: 1132758-31-6
(S)-N-(1-m-tolylpropan-2-yl)acetamide

Guidance literature:: With (1S,1'S,2R,2'R)-(+)-1,1'-di-t-butyl-[2,2']-diphospholane(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; hydrogen; In ethyl acetate; at 20 ℃; for 20h; under 22502.3 Torr; optical yield given as %ee; enantiospecific reaction; Inert atmosphere;
DOI:10.1002/anie.200805058

Reference yield:

: 18826-61-4
3-methylphenylacetone

: 108-24-7
acetic anhydride

: 1132758-31-6
(S)-N-(1-m-tolylpropan-2-yl)acetamide

: C₁₂H₁₇NO

Guidance literature:: 3-methylphenylacetone; With pyridoxal 5'-phosphate; amine transaminase ATA-415; isopropylamine; In aq. phosphate buffer; at 30 ℃; for 24h; pH=7.5; Enzymatic reaction;

acetic anhydride; enantioselective reaction;
DOI:10.1002/adsc.201900179

Reference yield:

: 3333-20-8
1-allyl-3-methylbenzene

: 1132758-31-6
(S)-N-(1-m-tolylpropan-2-yl)acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium 2,2,2-trifluoroacetate; iron(III) sulfate; palladium(II) trifluoroacetate / acetonitrile; water / 30 °C / Inert atmosphere; Darkness

2: pyridoxal 5'-phosphate; isopropylamine; amine transaminase TA-P₁-G₀₆ / aq. phosphate buffer / 24 h / 30 °C / pH 7.5 / Enzymatic reaction

With iron(III) sulfate; palladium(II) trifluoroacetate; pyridoxal 5'-phosphate; amine transaminase TA-P₁-G₀₆; sodium 2,2,2-trifluoroacetate; isopropylamine; In aq. phosphate buffer; water; acetonitrile; 1: |Wacker-Tsuji Olefin Oxidation;
DOI:10.1002/adsc.201900179